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A G Wintle

Publications and source records attributed to A G Wintle.

6 recordsLinked to original sources

Optical dating of dune sand from Blombos Cave, South Africa: I--multiple grain data.

An aeolian sand unit overlies the Middle Stone Age deposits at Blombos Cave on the southern Cape coast. These deposits contained culturally-important artefacts, including bone tools and pieces of engraved ochre, as well as a large number of worked lithics. The aeolian sand and two other remnants of the sand dune formed against the coastal cliff were dated using optical dating. To determine the dose received since deposition, measurements were made on 5mg aliquots of purified quartz grains using the single-aliquot regenerative-dose (SAR) protocol. The results of several internal check procedures are reported and at least 15 replicate dose determinations are presented for each sample. Combining these dose values with measurements of the radioactive content of each sample resulted in an age of 69.2+/-3.9 ka for the unit within the cave, and a mean age of 70.1+/-1.9 ka for all three dune samples. This provides a minimum age for the Middle Stone Age material at Blombos Cave.

Geologic Sediments↗

Optical dating of dune sand from Blombos Cave, South Africa: II--single grain data.

A sequence of optically stimulated luminescence measurements was made on each of 8,961 grains from three sand samples from Blombos on the southern Cape coast. One sand unit overlay Middle Stone Age deposits in Blombos Cave. The measurement sequence, the single aliquot regenerative dose protocol, was used to obtain values for the total effective radiation dose to which each grain had been exposed since burial. A series of checks was carried out on each grain to ensure that the luminescence signals were reproducible, and that they were derived from quartz. This led to acceptance of less than 5% of the grains. An estimate of the radiation dose for the sand unit was obtained by combining the values using the central age model. In order to use a larger number of grains that might be representative of the sand unit, the radiation dose was also estimated by using the signal from the above grains, combined with the signals from those grains that had lower signals, but nonetheless contributed to the total light sum; this utilised between 9 and 18% of the grains. This enables us to obtain estimates of the ages as 67.3+/-3.8 ka, 65.6+/-2.8 ka and 68.8+/-3.0 ka for the three samples. These values agree with ages obtained using the single aliquot regenerative dose protocol for aliquots composed of several hundred grains.

Dose-Response Relationship, Radiation↗

Retrospective dose assessment: the measurement of the dose in quartz in dating and accident dosimetry.

In retrospective dosimetry using luminescence it is never possible to obtain a sample of the unaltered phosphor as it was at somc time in the past and before radiation exposure. This prevents direct calibration using conventional personnel dosimetry techniques, and so measurement protocols must be devised which allow accurate estimation of the dose using only the exposed phosphor. This has led to the use of complex protocols, requiring many tens of notionally identical subsamples, to obtain one estimate of the unknown dose. More recently, considerable effort has gone into devising protocols which provide an estimate of the unknown dose from only one subsample. These avoid the need to assume homogeneity in the sample. These protocols also allow faster measurement, which for the first time makes it practical to obtain multiple estimates of the unknown dose and thus externally calculated random errors. This paper discusses the development of single-aliquot protocols, with particular reference to those devised for use with quartz, and finally reviews some of their applications in the retrospective assessment of dose.

Calibration↗

Electron-trapping probability in natural dosemeters as a function of irradiation temperature.

The electron-trapping probability in OSL traps as a function of irradiation temperature is investigated for sedimentary quartz and feldspar. A dependency was found for both minerals; this phenomenon could give rise to errors in dose estimation when the irradiation temperature used in laboratory procedures is different from that in the natural environment. No evidence was found for the existence of shallow trap saturation effects that could give rise to a dose-rate dependency of electron trapping.

Aluminum Silicates↗

Dose estimation using quartz OSL in the non-linear region of the growth curve.

The reliability of equivalent-dose determinations on quartz made with the single-aliquot regenerative-dose (SAR) protocol is examined using a suite of sedimentary samples for which the equivalent dose is expected to be >200 Gy. Experiments on one sample were used to evaluate the precision obtained using the standard measurement procedure with (a) a range of pre-heat temperatures, and (b) a single pre-heat temperature. The precision is compared with that achieved using SAR for a repeated dose point after an initial pre-heat, and for a known dose given before the initial pre-heat. It is concluded that, at least for this sample, the scatter in OSL measurements dominates the spread in the estimates of De.

Luminescent Measurements↗