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C Lennartz

Publications and source records attributed to C Lennartz.

3 recordsLinked to original sources

Individually selecting multi-reference CI and its application to biradicalic cyclizations.

In the present review a new algorithm to perform individually selecting MR-CI calculations is discussed. The new algorithm exploits the advantages arising from the subdivision of the molecular orbitals (MOs) into an internal and an external part and avoids the recalculation of representation matrices by the use of a specially designed cache. With the new algorithms we are able to perform calculations including more than 10 million selected configurations state functions (CSFs) as a matter of routine. As an example for the possibilities of the new approach the regioselectivity of thermal biradical cyclizations (C2-C7 vs. C2-C6 cyclization) is investigated in the second part of the present work. After studying the accuracy of various quantum chemical methods (MR-CI, density functional theory, and coupled cluster approaches) using (Z)-1,2,4 Heptatriene-6-yne as a model system the influence of substituents (R = H, Ph, t-Bu, NH2) on the regioselectivity is investigated. Our results rationalize the switch between the two biradical cyclizations on the basis of mainly steric (t-Bu) or electronic (Ph) substituent effects. Moreover, the results for R = NH2 predict that the activation energy of the C2-C6 cyclization can be lowered even more. However, a change in the reaction mechanism is found.

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New dyes based on amino-substituted acridizinium salts--synthesis and exceptional photochemical properties

The novel amino-substituted acridizinium salts 5a and 5b represent a new class of cyanine dyes which exhibit intense color along with efficient fluorescence properties. These dyes show moderate solvatochromism in their absorption and emission spectra. The absorption and emission shifts of the two chromophores display a reasonable correlation with solvent parameters such as donor and acceptor number. It was found that the dyes 5a and 5b interact with DNA, with quenching of the band intensies accompanied with a red shift of the absorption and emission bands. Moreover, irradiation of salts 5a and 5b in the presence of DNA results in DNA damage. Solution photolysis of acridizinium salt 5a gave the head-to-tail dimers as the major products (>95%), whereas the acridizinium salt 5b afforded the anti-head-to-tail dimer along with both head-to-head isomers. The latter are thermally labile and rapidly revert to the monomer.

Journal Article↗