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Biomedical subjects

C W Fairhurst

Publications and source records attributed to C W Fairhurst.

At least 19 recordsLinked to original sources
PubMed1995

Cyclic fatigue of a model feldspathic porcelain.

OBJECTIVES: This study was conducted to evaluate the fatigue parameters of a model porcelain based on the Weinstein patent using cyclic fatigue and to compare the parametric values obtained from cyclic fatigue tests with those from dynamic fatigue tests previously reported by Fairhurst et al. (1993). METHODS: Cyclical biaxial flexure of 1 mm thick and 12 mm diameter disks was performed at 37 degrees C in distilled water at a frequency of 4 Hz with constant stressing rates between a minimum and maximum stress. Three groups of samples (50, 40, 40) were tested with a maximum stress of 51, 47, and 43 MPa, respectively. The crack growth exponent, n, and the scaling constant, sigma fo, were derived from the regression constants obtained from a linear regression of the logarithm of the median time to failure with the logarithm of the maximum stress. RESULTS: No significant differences were found between the cyclic fatigue parameters, n and sigma fo, derived from the median time to failure and those obtained from dynamic fatigue data. SIGNIFICANCE: Within the limits of error in this determination, the median cyclic fatigue life can be estimated by the use of fatigue parameters obtained from dynamic fatigue testing.

Analysis of Variance↗
PubMed1993

Effect of Griffith precracks on measurement of composite fracture toughness.

The objective of this study was to produce true Griffith-type cracks in composite specimens for measuring fracture toughness. A compact test specimen geometry, conforming to the ASTM standard (E-399-84) was chosen for the evaluation. Five methods of precracking were evaluated: 1) placing no precrack (notch in specimen left blunt); 2) placing a sharp notch with a Bard Parker blade under hand pressure; 3) placing a sharp notch with a Bard Parker blade under hand pressure, followed by stressing the sample at 60% of the failure load for 25 cycles; 4) forming a sharp notch by placing a razor blade in the sample during polymerization; and 5) placing a Griffith-type crack. Results indicate that the method of precracking a sample does have a significant effect on the measured value of the fracture toughness.

Analysis of Variance↗
PubMed1993

Dynamic fatigue of feldspathic porcelain.

Several studies (Sherrill and O'Brien, 1974; Southan and Jørgensen, 1974; Jones, 1983) have shown that stress corrosion fatigue occurs in dental porcelains. Morena et al. (1986) reported on an assessment of slow crack growth parameters for dental ceramics. The purpose of the study reported here was to evaluate the fatigue parameters of a model experimental porcelain using dynamic fatigue testing. This test procedure makes use of several constant stressing rates to perform strength tests. Dynamic stress testing was first described by Evans (1974) and later defined as a distinct test modality by Ritter (1978). From such data, the fatigue parameters can be calculated. These fatigue parameters, n and sigma f0, are, respectively, the crack growth exponent from the crack velocity expression and a materials constant which is dependent on the test environment and the inert (moisture-free) strength. The model porcelain was made from 60% component 1 and 40% component 3 according to the Weinstein patent (Weinstein, et al., 1962). The biaxial flexure strength of 300 specimens 1 mm thick was tested in 37 degrees C water by testing 50 samples at each of 6 constant stressing rates: 100, 10, 1, 0.1, 0.01, and 0.001 MPa/s. One hundred specimens were tested in a moisture-free environment at 100 MPa/s using a servo-mechanical testing machine. A commercial porcelain (Jelenko Gingival-Lot # 2012, Jelenko Dental Health Products, Armonk, NY, USA) was chosen as a reference material. One hundred twenty specimens were tested using the same procedures as those used for the model porcelain; however, only 20 samples were tested for 5 stressing rate groups and an inert group.(ABSTRACT TRUNCATED AT 250 WORDS)

Aluminum Silicates↗
PubMed1992

The effect of glaze on porcelain strength.

The self-glazing technique provides an esthetic and hygienic surface for crowns and fixed partial dentures that use porcelain veneers. A study of the biaxial flexure strengths of polished vs. glazed specimens is needed to verify that current laboratory methods are appropriate for planned fatigue studies. Four groups of 50 porcelain disk specimens each were subjected to the following polishing and firing procedures: group one was fired, glazed-no hold, and polished; group two was fired, polished, and glazed-no hold; group three was fired, polished and glazed-1 min. hold; group four was fired, polished, and not glazed. The piston-on-three-ball method was used for testing biaxial flexure strengths. Significantly lower differences in biaxial flexure strengths were noted when group two values were compared with values from groups one, three and four. The results show that the Weibull distribution is an appropriate model for our studies. Differences in glaze thickness among the groups were noted in SEM examination; however, bulk (interior) microcrack density differences were absent. The specimens that were fired, polished to a 1 micron surface finish, and not glazed (group four) were significantly higher in flexure strength than groups one and three at the p less than 0.001 level. The hypothesis that glazing of porcelain surfaces improves the biaxial flexure strength of test specimens was rejected.

Dental Casting Technique↗
PubMed1992

Dental ceramics: the state of the science.

This review covers the properties of dental ceramics. Castable systems, bioactive glass, PMF systems, CAD/CAM, and ceramic brackets in orthodontics are briefly discussed. Many of the advances made between 1960 and 1975 were directed toward the understanding, controlling, and developing of new ceramic processes. New and deeper understanding of the structure of non-crystalline solids, structural imperfections, sintering physics, and other physical phenomena related to the melting and solidification processes has brought ceramics from the near-total art form process of the mid-century to the status of a highly sophisticated science it enjoyed in the 1980's.

Aluminum Oxide↗
PubMed1991

Fracture durability of restored functional cusps on maxillary nonvital premolar teeth.

Palatal cusps of nonvital maxillary premolar teeth were restored with a coronal-radicular restoration of posterior composite resin (Occlusin), amalgam (Tytin), or cermet (Chelon-Silver). Mean fracture strength values were: 370 lb for intact premolar teeth, 266 lb for amalgam, 215 lb for posterior composite resin, and 132 lb for cermet. From this in vitro study it can be suggested that for selected endodontically treated maxillary premolar teeth, the dentist can use acid-etch-retained posterior composite resin or pin-retained high copper amalgam material for a definitive coronal-radicular restoration. The use of cermet for this purpose is contraindicated.

Bicuspid↗
PubMed1991

Effects of specimen geometry on the measurement of fracture toughness.

The objective of this study was to investigate the use of compact test specimen geometries of reduced size for the measurement of fracture toughness, KIc, of dental resin composites. Provisional fracture toughness values were determined for four dental composites by use of a reduced-size compact test specimen. The specimens were volumetrically 8% of the size of compact test specimens used in previous studies on dental composites. The test results and conditions met validity tests. These results were compared with those from previous studies that used large compact test specimens. It is concluded that the reduced-size compact test specimen is an acceptable alternative for measurement of fracture toughness.

Acrylic Resins↗
PubMed1990

Calibration of FTIR conversion analysis of contemporary dental resin composites.

Composite restorative material has undergone gradual change in composition since its introduction in the 1960's. Early commercial resins were mixtures of BIS-GMA and TEGDMA. Today, these mixtures are still present, but urethane dimethacrylates and large oligomeric structures of BIS-GMA-urethanes exist. Because of these changes in composition, the past methods of calculating monomer conversion by means of infrared spectroscopy may need modification. This research investigates different methods used to formulate calibration curves for determination of monomer conversion by infrared spectroscopy of contemporary commercial composites containing aromatic structures. Conversion calibration procedures using various baseline methods with BIS-GMA, Bisphenol-A/TEGDMA, and a hydrogenated bonding resin were established. Both peak and area infrared absorptions were determined. One particular baseline method proved the best fit to the Beer-Lambert law. Bisphenol-A was found unsuitable as an infrared calibration model for resin composites. The BIS-GMA/TEGDMA calibration model closely simulates conversion values obtained when a hydrogenated commercial resin model was used.

Analysis of Variance↗
PubMed1990

Oxide adherence and porcelain bonding to titanium and Ti-6Al-4V alloy.

The bonding of an experimental low-fusing porcelain to titanium and Ti-6Al-4V was evaluated by an x-ray spectrometric technique that measures the area that remains covered with porcelain following a controlled deformation of the metallic substrate. Oxide adherence strength values for titanium and Ti-6Al-4V oxidized at 750 degrees and 1000 degrees C were measured in tension with use of high-strength adhesives. The effect of further oxidation that would occur during porcelain firing was evaluated via simulated porcelain firings without actual porcelain application. Interface cross-sections of the titanium-porcelain and Ti-6Al-4V-porcelain bonds were examined in a scanning electron microscope (SEM). The porcelain was found to delaminate completely from the metal substrate, leaving less than 1% of the surface covered with porcelain. The oxide adherence of the specimens oxidized at 750 degrees C was good, but those oxidized at 1000 degrees C exhibited significantly lower oxide adherence (p = 0.001). The simulated porcelain-firing oxidation treatments also produced a significant decrease in oxide adherence (p = 0.004). The 750 degrees C oxidation treatments produced oxide films too thin to be visualized in the SEM, whereas the 1000 degrees C oxidation treatments produced oxide films approximately 1 micron thick. The lower oxide adherence of the 1-micron-thick oxide films is consistent with reports in the titanium literature of oxide delamination when the oxide film reaches 1 micron in thickness.

Alloys↗
PubMed1989

The effect of thermal history on porcelain expansion behavior.

Porcelain-fused-to-metal restorations are fixed several hundred degrees above the glass-transition temperature and cooled rapidly through the glass-transition temperature range. Thermal expansion data from room temperature to above the glass-transition temperature range are important for the thermal expansion of the porcelain to be matched to the alloy. The effect of heating rate during measurement of thermal expansion was determined for NBS SRM 710 glass and four commercial opaque and body porcelain products. Thermal expansion data were obtained at heating rates of from 3 to 30 degrees C/min after the porcelain was cooled at the same rate. By use of the Moynihan equation (where Tg systematically increases in temperature with an increase in cooling/heating rate), the glass-transition temperatures (Tg) derived from these data were shown to be related to the heating rate.

Chemical Phenomena↗
PubMed1989

A rapid heating and cooling rate dilatometer for measuring thermal expansion in dental porcelain.

Herein we describe a dilatometer that consists of a low-mass infrared furnace for rapid heating or cooling, an optical pyrometer, and a laser interferometer. The dilatometer facilitates observations of thermal expansion at rates comparable with those in dental laboratory practice over the temperature range necessary for comparison of thermal expansion of dental porcelain and alloy. Examples of thermal expansion data obtained at a 600 degrees C/min heating rate on NIST SRM 710 glass and dental porcelain are reported. To a limited extent, thermal expansion data above the glass-transition temperature range of dental porcelain were obtained. A shift of the glass-transition temperature range to higher temperatures was observed for both materials, compared with data obtained at 20 degrees C/min.

Chemical Phenomena↗
PubMed1988

The relationship between oxide adherence and porcelain-metal bonding.

The lack of a reliable bond test has hindered the elucidation of the mechanism for porcelain-metal bonding in dental systems, because a test capable of detecting differences among porcelain-metal bonds of various qualities is required before the reasons for these differences may be ascertained. A method was developed in the present study whereby specimens of alloys with differing physical properties may be deformed to a constant strain to yield a fracture surface suitable for measurement of the area fraction of retained porcelain by an x-ray spectrometric technique described previously. The method proved sufficiently discriminating that significant differences could be found in 48 of the possible 66 comparisons among alloys and treatments. Linear regression analysis revealed a strong correlation (r2 = 0.947) between the area fractions of retained porcelain measured in the present study and the oxide adherence strength values measured previously. This strong correlation, when considered in light of the literature evidence for the presence of an oxide layer at the porcelain-metal interface, provides compelling support for the oxide layer theory of porcelain-metal bonding in dental alloy systems.

Dental Bonding↗
PubMed1988

Microleakage of root restorations.

This study evaluated the microleakage of various restorative materials placed in root surfaces. A minimum of 20 freshly extracted single-rooted teeth were used for each combination of restorative materials. Four preparations were made on the root surface and each restored with a different material. After thermocycling in dye, the root was cut transversely in several sections through the restoration, and microscopically examined to record the microleakage at the interface between restorative materials and tooth. Results indicated that fewer composite resin specimens allowed microleakage into dentin as compared with either amalgam or glass ionomer materials.

Composite Resins↗
PubMed1986

Glass transition temperatures of dental porcelains at high heating rates.

The glass transition temperature (Tg) of a dental porcelain is a factor in determining the magnitude of residual stresses introduced in a dental porcelain during cooling of a porcelain-fused-to-metal prosthesis. Tg is known to vary with changes in heating or cooling rate. However, available commercial instrumentation does not permit Tg to be obtained at the very high cooling rates commensurate with actual dental laboratory practice. Tg values are reported here for a number of commercial dental porcelains and other materials. These data were obtained by the bending beam technique, employing a special low thermal-mass furnace to permit rapid heating and cooling rates. Measurements were made at rates as high as 600 degrees C/min. Coefficients of determination (r2) for 1/Tg vs. ln (heating rate) were excellent. This relation is consistent with previously reported low rate Tg data obtained by a different technique.

Dental Porcelain↗
PubMed1986

Fatigue of dental ceramics in a simulated oral environment.

Fatigue in ceramics refers to the subcritical growth of cracks, aided by the combined influence of water and stress. The dynamic fatigue (constant stressing rate) method was used to obtain subcritical crack growth parameters for three dental ceramics: a feldspathic porcelain, an aluminous porcelain, and a fine-grain, polycrystalline core material. The constant stressing rate experiments were carried out at 37 degrees C for all three ceramics in distilled water, and, for the feldspathic porcelain, in artificial saliva as well. Considerable differences were found in the value of the crack growth exponent (n) among the three ceramics. The feldspathic porcelain was lowest in n-value, while the fine-grain ceramic had the highest n-value. No differences were found for the feldspathic porcelain with respect to n measured in water and in the artificial saliva. Lifetime prediction curves in 37 degrees C water, constructed from the n-values and inert strengths, showed that fatigue failure within five years is a good possibility for feldspathic porcelain specimens at stress levels which can reasonably be anticipated to occur in the oral environment. Little likelihood of failure was perceived for the fine-grain ceramic. The aluminous porcelain was intermediate between these two materials with respect to failure probability.

Dental Porcelain↗