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Biomedical subjects

Franklin Tay

Publications and source records attributed to Franklin Tay.

7 recordsLinked to original sources

Immediate and 24-hour evaluation of the interfacial strengths of fiber posts.

This study examined the contribution of testing time on the interfacial strengths of fiber posts to radicular dentin. Twenty-five fiber posts were luted to root segments with resin cements and a zinc phosphate cement. Immediately upon setting of the materials, the roots were sectioned into slices and randomly divided into two subgroups, depending on testing time (immediate vs. 24-hours), for push-out test. The results showed an improvement on the interfacial strength after 24 hours of storage. When data were pooled for each cement, the interfacial strengths (MPa) were: Optibond Solo Plus/Nexus: 10.3+/-3.8a; zinc phosphate cement: 10.1+/-2.7a; Multilink: 9.6+/-3.8ab; RelyX Unicem: 7.1+/-4.9bc; AllBond 2/Duolink: 6.7+/-3.5c (groups with same superscript letter were not statistically significant). It is concluded that bond strength can increase during the first 24 hours and that the interfacial strength is predominantly contributed by frictional retention.

Analysis of Variance↗

Durability of resin-dentin bonds: effects of direct/indirect exposure and storage media.

OBJECTIVES: To evaluate the longevity of resin-dentin bonds of three adhesives using different storage media and specimen size. METHODS: Flat dentin surfaces from extracted human third molars were bonded with: a two-step etch-and-rinse self-priming adhesive (Single Bond), a two-step self-etching adhesive (Clearfil SE Bond), and a one-step self-etching adhesive (One-Up Bond F). Composite build-ups were constructed. The bonded teeth were stored under three conditions: dry, distilled water, or mineral oil. Half of the specimens were stored as intact bonded teeth (Indirect Exposure/IE). The other half were first sectioned into beams and stored under same conditions (Direct Exposure/DE). After storage periods of 24h, 3 months or 1 year, the intact teeth (IE) were sectioned into beams and both subgroups (DE and IE) were tested for microtensile bond strengths. Results were analyzed with multiple ANOVA and Student-Newman-Keuls tests. Fractographic analysis was performed by SEM. RESULTS: After 24h, Single Bond and Clearfil SE Bond performed equally and were superior to One-Up Bond F. After 3 months of DE to water storage, decreases in bond strengths were observed for Single Bond and One-Up Bond F, this decrease occurred for Clearfil SE Bond after 12 months of water storage. Bonded specimens aged in dry did not alter bond strengths over time. Bond strength increased when Single Bond was stored in mineral oil after 3 and 12 months. Micromorphological alterations were evident after water storage. SIGNIFICANCE: Although dentin bond strength of all the adhesives fell over time in DE, SE Bond fells the least.

Acid Etching, Dental↗

Evaluation of the effect of water-uptake on the impedance of dental resins.

UNLABELLED: Electrical impedance spectroscopy (EIS) offers a quantitative method of measuring the stability of resin films in aqueous solution over time. PURPOSE: The purpose of this study was to measure the EIS of five experimental dental adhesive films (ca. 17 microm thick) of increasing hydrophilicity (ranked by their Hoy's solubility parameters), and how much these values change over 3 weeks in aqueous buffer. METHODS: The resin films were placed in a U-shaped chamber and a pair of Ag-AgCl electrodes was used for EIS. The EIS results were confirmed by immersing the films in 50% AgNO3 for 24 h to trace the distribution of any water absorption into the resins by TEM observations. RESULTS: The resistance (Rr) of the resins 1-4 films increased most during the first day, and varied from 1x10(11) ohm for resin 1, to 40Omega for resin 5 at day 1. The day 1 Rr values of resins 1-4 were inversely proportional to their Hoy's solubility parameter for hydrogen bonding forces. Electrical impedance values of resins 1-3 and 5 varied widely but were relatively constant over time, while those of resin 4 decreased more than 99% from day 1 to 21 (p<0.05). Capacitance (Cr) of films of resins 1-4 all increased over the first day and then were relatively unchanged over the 20 days (except for resin 4 that continued to increase) and were between 0.01 and 1 nF. Silver uptake by TEM revealed the development of water-filled branching structures that formed in resins 4 and 5 over time.

Adhesives↗

The adhesion between fiber posts and root canal walls: comparison between microtensile and push-out bond strength measurements.

Aim of the study was to compare the trimming and non-trimming variants of the microtensile technique with the 'micro' push-out test in the ability to measure accurately the bond strength of fiber posts luted inside root canals. In 15 endodontically treated teeth (Group A), fiber posts were cemented with Excite DSC in combination with Variolink II (Ivoclar-Vivadent). In 15 roots RelyX Unicem (3M-ESPE) was used for fiber post luting (Group B). Within each group, the bond strength of cemented fiber posts was assessed with the trimming and non-trimming microtensile technique, as well as with the push-out test. The great number of premature failures (16.9% in Group A, 27.5% in Group B) and the finding of high standard deviation values make questionable the reliability of the trimming microtensile technique. With the non-trimming microtensile technique, only five sticks were obtained from a total of six roots. The remaining specimens failed prematurely during the cutting phase. With the push-out test no premature failure occurred, the variability of the data distribution was acceptable, and regional differences in bond strength among root levels could be assessed. Relatively low values of bond strength were, in general, recorded for luted fiber posts. In conclusion, when measuring the bond strength of luted fiber posts, the push-out test appears to be more dependable than the microtensile technique.

Dental Bonding↗

Microleakage and interfacial morphology of self-etching adhesives in class V resin composite restorations.

The purpose of the study was to evaluate the marginal leakage of three adhesive systems in Class V resin composite restorations. Two adhesive systems containing acidic primers: Clearfil SE Bond (CSEB) and Etch & Prime 3.0 (E&P), were compared with a conventional water-based primer: Scotchbond Multipurpose Plus (SBMP). Class V cavities were made at the cementum-enamel junction of extracted human molars, which were then divided between three groups. One of the adhesive systems was applied to each group following manufacturers' instructions. Composite restorations were placed, light cured for 40 s, and polished. Specimens were then immersed in a solution of 2% basic fuchsin dye for 24 h. Longitudinal sections were obtained and studied with a stereomicroscope for assessment of the microleakage according to the degree of dye penetration (scale of 0-3). Data were analyzed by Kruskal-Wallis one-way ANOVA, Mann-Whitney tests, and the Wilcoxon matched-pairs signed rank test. Two specimens for each group were analyzed by scanning-electron microscopy (SEM). Bonded interfaces of dentin were also examined by transmission-electron microscopy (TEM). On enamel, there were no significant differences between the three groups. On dentin, CSEB showed the lowest dye penetration values among the three adhesive systems. SEM and TEM studies showed hybrid layer and resin tag formations in all groups.

Acid Etching, Dental↗

Dentin deformation after scratching with clinically-relevant forces.

OBJECTIVE: In order to understand the mechanism of dentin sensitivity to tactile stimuli, the purpose of this study was to evaluate possible permanent deformation of dentin produced by scratching dentin surfaces with clinically-relevant forces. METHODS: Midcoronal dentin was prepared from twenty human teeth and polished to 4000-grit and ultrasonicated. The dentin surface of each specimen was scratched under forces ranging from 30 to 100 centi-Newtons (cN). The depth of the grooves were measured with a profilometer and the overall hardness of dentin in the vicinity of the grooves was measured. Additional dentin specimens were prepared for SEM evaluation. RESULTS: Dentin hardness was constant and no statistical difference was found among the specimens. Statistically significant differences in groove width and depth were found when increasing force was applied to the dental explorer tip. The depth of the groove ranged from 0.21+/-0.09 microm for the 30 cN group to 1.27+/-0.39 microm for the 100 cN group. The width of the groove ranged from 19.3+/-4.0 microm for the 30 cN group to 43.0 microm for the 10 0 cN group. CONCLUSIONS: (1). The threshold force necessary to create scratches in dentin with a dental explorer was 30 cN or a compressive stress of 1003 MPa. As this exceeds the crushing strength of dentin, this force produces plastic deformation of dentin; (2). Theoretical calculations indicated that even the highest scratching forces (100 cN) could not induce sufficient fluid flow to activate pulpal mechanoreceptors, although it could induce sufficient elastic deformation to theoretically shift dentinal fluid at a rate sufficient to activate mechanoreceptors; (3). The results of this work may lend support the hydrodynamic theory in that scratching of dentin surfaces causes both elastic and plastic deformation of dentin that may displace dentinal fluid toward the pulp where it could activate mechanoreceptors.

Dentin↗

Effect of sodium hypochlorite on dentin bonding with a polyalkenoic acid-containing adhesive system.

The purpose of this study was to evaluate the effect of sodium hypochlorite (NaOCl) treatment on dentin bonding by means of contact angle (CA), shear bond strength (SBS), and microleakage (ML) measurements. Ultrastructure and nanoleakage (NL) of the interfaces were examined by transmission electron microscopy (TEM). For CA, SBS, and TEM evaluation, human molars were sectioned to expose dentin surfaces and were either acid-etched (35% H3PO4) or further treated with 5% NaOCl for 2 min before the application of Single Bond adhesive. CAs were measured using the Axisymmetric Drop Shape Analysis technique. The Watanabe testing assembly was used for SBS evaluation. ML was assessed by a dye penetration method. NL was examined using a silver-staining technique. The results showed that CA values decreased after acid etching and even more after NaOCl treatment. NaOCl treatment produced lower SBS than acid-etched dentin. Both ML values and NL manifestations were similar for NaOCl-treated and acid-etched dentin. NaOCl did not completely remove the collagen matrix. NL was manifested along the base of hybrid layers and within the polyalkenoic acid copolymer in both groups. Adverse chemical interactions could have occurred between the remnant collagen matrix and/or mineralized dentin after NaOCl treatment. There is no additional advantage in using NaOCl treatment with this adhesive.

Alkenes↗