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J Colmenero

Publications and source records attributed to J Colmenero.

33 records · Page 2Linked to original sources
PubMed1998

Investigation of the Dielectric beta-Process in Polyisobutylene by Incoherent Quasielastic Neutron Scattering.

Recently by dielectric spectroscopy a new secondary relaxation process in polyisobutylene (PIB) was detected showing all the signatures of a Johari-Goldstein relaxation [Richter, D; Arbe, A.; Colmenero, J.; Monkenbusch, M.; Farago, B.; Faust, R. Macromolecules 1998, 31, 1133]. Using high resolution neutron backscattering, we investigated the quasielastic neutron spectra from protonated PIB which are related to this process as a function of momentum transfer and temperature. In addition we studied the elastically scattered intensity over a wide temperature range. After multiple scattering corrections all results can be described consistently in terms of a local jump process with the distribution parameters from the dielectric beta-relaxation. The spatial extent of the associated protonic motion was determined to be d = 2.7 Å. A comparison with the existing body of data for PIB leads to the conclusion that the dielectric beta-process and the earlier found delta-process must be identical, thereby revising the assignment of the delta-process as due to methyl group rotation. Finally, we remark on aspects of the relation between quasielastic coherent and incoherent scattering and address the seemingly contradictory result of different length scales revealed for the same process with the two techniques.

Journal Article↗
PubMed1990

Multicenter prospective study of treatment of Brucella melitensis brucellosis with doxycycline for 6 weeks plus streptomycin for 2 weeks.

The effectiveness of treating human brucellosis caused by Brucella melitensis with a 6-week course of doxcycline plus streptomycin for 2 of those weeks was analyzed by a multicenter prospective study of 139 patients. Subjects with central nervous system involvement, endocarditis, or spondylitis were excluded from the study. All but 5 of the 139 patients completed the full treatment schedule and became afebrile in the first week of therapy. Four patients suffered relapses during the follow-up period. Of the five patients who did not complete the treatment, two left because of adverse secondary effects (1.4%), another two left for noncomplicance with the treatment (1.4%), and the remaining patient was considered a therapeutic failure because his symptoms persisted after the first week of therapy (0.7%). We concluded that the combination of doxycycline and streptomycin is an effective treatment for the types of brucellosis included in our study.

Adolescent↗