Advancing hyphenated chromatographic systems
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Biomedical subjects
JC Lindon
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Three-dimensional maximum-quantum correlation HMQC NMR spectroscopy (3D MAXY-HMQC)
The extension of two-dimensional maximum-quantum correlation spectroscopy (2D MAXY NMR), which can be used to simplify complex NMR spectra, to three dimensions (3D) is described. A new pulse sequence for 3D MAXY-HMQC is presented and exemplified using the steroid drug dexamethasone. The sensitivity and coherence transfer efficiency of the MAXY NMR approach has also been assessed in relation to other HMQC- and HSQC-based 3D methods. Copyright 1997 Academic Press. Copyright 1997Academic Press
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