Metal oxide monolithic columns.
Metal oxide monoliths composed of ZrO2 and HfO2 have been synthesized in situ inside capillary columns. The material shows globular-like structure and through pores. Capillary electrochromatography and capillary liquid chromatography were performed in a monolithic column with the HfO2 material. Separation of a simple sample mixture showed the potential of the new metal oxide monolithic columns.