Biomedical subjects

Marcelo Ferraz Mesquita

Publications and source records attributed to Marcelo Ferraz Mesquita.

9 recordsLinked to original sources

PubMed2006

Effect of water storage on tooth displacement in maxillary complete dentures.

The purpose of this study was to investigate the effect of water storage at 37 degrees C (1 week, 1 month and 3 months) on tooth displacement in maxillary complete dentures. Ten maxillary dentures were constructed with Clássico acrylic resin using the conventional method of packing in metallic flasks. Metallic reference pins were placed in the incisal border of the central incisors (I), labial cusp of the first premolars (PM), and mesiolabial cusp of the second molars (M). Twelve hours after final flask closure, the acrylic resin was cured in water at 74 degrees C for 9 h. The flasks were removed from the thermo-polymerizing unit after water-cooling and the dentures were deflasked, finished and stored in water at a temperature of 37 degrees C for 1 week, 1 month and 3 months. At deflasking and at the water storage intervals, the I-I (incisor to incisor), PM-PM (pre-molar to pre-molar), and M-M (molar to molar) transversal distances, and LI-LM (left incisor to left molar) and RI-RM (right incisor to right molar) anteroposterior distances were measured using an optical microscope with 0.0005 mm accuracy. Data were submitted to ANOVA and Tukey's test (5%). Comparing the evaluation periods for each individual transversal and anteroposterior reference point, no statistically significant differences were observed among deflasking and the water storage intervals for I-I, PM-PM, M-M and RI-RM distances (p>0.05). For LI-LM, however, deflasking values were statistically different from those of 1-week, 1-month and 3-month water storage intervals (p<0.05), which, in turn, did not differ statistically to each other (p>0.05). These results confirm the complexity of tooth displacement in complete dentures. From a clinical standpoint, the difference observed in LI-LM distance after water storage would not be detected by the patients during clinical use.

Dentures↗

PubMed2006

Over-refractory casting technique as an alternative to one-piece multi-unit fixed partial denture frameworks.

STATEMENT OF PROBLEM: Soldering has been suggested to achieve acceptable fit of multi-unit fixed partial denture (FPD) frameworks of 3 or more elements. However, distortion of the entire framework may occur. PURPOSE: The purpose of this study was to evaluate marginal fit in 1-piece-casting FPD frameworks comparing 2 casting techniques: the conventional technique (CT) and the over-refractory technique (ORT). The techniques were evaluated on castings made from commercially pure titanium (CP Ti; Tritan), titanium-aluminum-vanadium (Ti-6Al-4V), and nickel-chromium (Ni-Cr; VeraBond II) alloys. MATERIAL AND METHODS: A metal master cast including 3 preparations was created to simulate a 5-unit FPD. The metal cast was duplicated in vinyl polysiloxane for fabrication of 60 working casts. For the CT, 0.7-mm-thick patterns were waxed on the casts using an electrical wax-dipping unit. Patterns were removed from the preparations before investing. For the ORT, the silicone impressions were poured with an investment material (Rematitan for CP Ti and Ti-6Al-4V, and Talladium for Ni-Cr). The patterns were waxed on the refractory casts, and the assembly was invested. Both CT and ORT (n = 10), CP Ti, and Ti-6Al-4V frameworks were cast using an arc-melting titanium vacuum-casting machine. The Ni-Cr frameworks were cast using an automated centrifugal-casting machine. The mean marginal discrepancies of the frameworks were measured at the mesial, distal, buccal, and lingual interfaces. Marginal gap measurements were recorded 3 times for each surface to the nearest 0.5 microm using a traveling microscope (x50). The data were analyzed with 2-way analysis of variance, followed by the Tukey HSD test (alpha=.05). RESULTS: Marginal discrepancies for the ORT specimens (82.8 +/- 1.7 microm for CP Ti; 64.4 +/- 1.3 microm for Ti-6Al-4V; and 77.2 +/- 1.5 microm for Ni-Cr) were significantly lower than those obtained for the CT specimens (106.3 +/- 2.6 microm for CP Ti; 75.7 +/- 0.8 microm for Ti-6Al-4V; 101.9 +/- 1.7 microm for Ni-Cr) (P < .05). For both techniques, marginal discrepancies were significantly different among the alloys evaluated, presenting the following order from greatest to least marginal discrepancy: CP Ti, Ni-Cr alloy, and Ti-6Al-4V (P < .05). CONCLUSION: The ORT for multi-unit FPD frameworks demonstrated significantly lower marginal discrepancies than the CT.

Alloys↗

PubMed2005

The influence of mold temperature on the fit of cast crowns with commercially pure titanium.

Commercially pure titanium (CP Ti) has been widely applied to fabricate cast devices because of its favorable properties. However, the mold temperature recommended for the manufacture of casts has been considered relatively low, causing inadequate castability and poor marginal fit of cast crowns. This study evaluated and compared the influence of mold temperature (430 degrees C--as control, 550 degrees C, 670 degrees C) on the marginal discrepancies of cast CP Ti crowns. Eight bovine teeth were prepared on a mechanical grinding device and impressions were used to duplicate each tooth and produce eight master dies. Twenty-four crowns were fabricated using CP Ti in three different groups of mold temperature (n = 8): 430 degrees C (as control), 550 degrees C and 670 degrees C. The gap between the crown and the bovine tooth was measured at 50 X magnification with a traveling microscope. The marginal fit values of the cast CP Ti crowns were submitted to the Kruskal-Wallis test (p = 0.03). The 550 degrees C group (95.0 microm) showed significantly better marginal fit than the crowns of the 430 degrees C group (203.4 microm) and 670 degrees C group (213.8 microm). Better marginal fit for cast CP Ti crowns was observed with the mold temperature of 550 degrees C, differing from the 430 degrees C recommended by the manufacturer.

Animals↗

PubMed2005

Influence of chemical and mechanical polishing on water sorption and solubility of denture base acrylic resins.

Influence of polishing methods on water sorption and solubility of denture base acrylic resins was studied. Eighty samples were divided into groups: Classico (CL), and QC 20 (QC) - hot water bath cured; Acron MC (AC), and Onda Cryl (ON) - microwave cured; and submitted to mechanical polishing (MP) - pumice slurry, chalk powder, soft brush and felt cone in a bench vise; or chemical polishing (CP) - heated monomer fluid in a chemical polisher. The first desiccation process was followed by storage in distilled water at 37 +/- 1 degrees C for 1 h, 1 day, 1, 2, 3 and 4 weeks. Concluding each period, water sorption was measured. After the fourth week, a second desiccation process was done to calculate solubility. Data were submitted to analysis of variance, followed by Tukey test (p<or=0.05). Means of water sorption (%) and solubility (%), respectively, were: CL-MP: 1.92 and 0.02; CL-CP: 1.98 and 0.52; QC-MP: 2.31 and -0.05; QC-CP: 2.32 and 0.25; AC-MP: 2.45 and -0.07; AC-CP: 2.43 and 0.41; ON-MP: 2.32 and -0.06; ON-CP: 2.34 and 0.27. Mechanical polishing promoted significantly lower solubility of acrylic resins; initially, water sorption values were higher for chemically polished samples, however, after 4 weeks all groups were similar.

Absorption↗

PubMed2005

Surface roughness and fatigue performance of commercially pure titanium and Ti-6Al-4V alloy after different polishing protocols.

STATEMENT OF PROBLEM: Surface quality of cast metal is directly related to service performance under fatigue stress. Surface heterogeneities resulting from either finishing or polishing processes or by corrosive agents such as fluoridated solutions, can negatively affect fatigue life. Cast titanium frameworks are difficult to polish, and an accepted polishing protocol has not been established. PURPOSE: This study evaluated and compared surface roughness of cast commercially pure titanium (CP Ti) and Ti-6Al-4V alloy submitted to conventional or electrolytic polishing, correlating the results with corrosion-fatigue strength testing performed in artificial fluoridated saliva. Specimens were also tested in air at room temperature to evaluate the effectiveness of the corrosion-fatigue test model. MATERIAL AND METHODS: For each metal, 40 dumb-bell-shaped rods, 2.3 mm in diameter at the central segment, were cast. Conventional polishing was performed on 20 specimens of each metal following the manufacturer's instructions. A source of continuous electrical current was used for electrolytic polishing of the other 20 specimens of each metal, which were immersed in an electrolytic solution containing 5% fluoridric acid, 35% nitric acid, and 60% distilled water. Surface roughness, Ra (microm), was measured with a profilometer, and fatigue tests were carried out with a universal testing machine using a load 30% lower than the 0.2% offset yield strength. After failure, the fractured surfaces were examined using scanning electron microscopy. Surface roughness means were analyzed with a 2-way analysis of variance and the Tukey multiple comparisons test (alpha=.05). RESULTS: Electrolytic polishing (0.24 +/- 0.05 microm) provided significantly (P <.05) lower surface roughness values than conventional polishing (0.32 +/- 0.06 microm). Regardless of the polishing protocol, surface roughness of Ti-6Al-4V alloy (0.25 +/- 0.06 microm) was significantly lower (P <.05) than that of CP Ti (0.31 +/- 0.05 microm), and the fluoridated environment did not influence fatigue performance. There was no correlation between fatigue performance and surface roughness. CONCLUSION: Surface roughness of Ti-6Al-4V was significantly lower than that of CP Ti. For cast titanium frameworks, the electrolytic polishing regimen was found to be more effective than the manufacturer's polishing instructions with abrasives and rotary instruments. After polishing, differences in surface roughness values did not affect corrosion-fatigue performance.

Alloys↗

PubMed2004

Effect of packing types on the dimensional accuracy of denture base resin cured by the conventional cycle in relation to post-pressing times.

This study investigated the dimensional stability of denture bases influenced by packing methods, in relation to post-pressing times, in the Clássico acrylic resin which was prepared according to manufacturer recommendations. Forty maxillary wax bases were made and randomly assigned into 2 groups of 20 specimens each according to the conventional and RS system packing methods. In each method, the specimens were subdivided into immediate, 6, 12 and 24 h post-pressing times. The dough of the acrylic resin was packed in metallic flasks and processed in a water bath curing cycle at 74 masculine C for 9 h. After cooling at room temperature, the bases were removed from the flasks, finished and fixed on stone casts with instantaneous adhesive. The resin base-stone cast sets were transversally sectioned into 3 sections and the base-stone gap measured at 5 points in each section. The data were submitted to ANOVA and Tukey's test, which showed that the RS system had a smaller base distortion compared to conventional packing, with the exception of the 24-h post-pressing time. There was a statistically significant difference between the packing methods only in section C (posterior palatal zone). In the conventional packing method, the immediate and 6 h times demonstrated values with no statistically significant difference between them, as well as between the 12 and 24 h post-pressing times.

Acrylic Resins↗

PubMed2004

Evaluation of varying amounts of thermal cycling on bond strength and permanent deformation of two resilient denture liners.

STATEMENT OF PROBLEM: Two problems found in prostheses with resilient liners are bond failure to the acrylic resin base and increased permanent deformation due to material aging. PURPOSE: This in vitro study evaluated the effect of varying amounts of thermal cycling on bond strength and permanent deformation of 2 resilient denture liners bonded to an acrylic resin base. MATERIAL AND METHODS: Plasticized acrylic resin (PermaSoft) or silicone (Softliner) resilient lining materials were processed to a heat-polymerized acrylic resin (QC-20). One hundred rectangular specimens (10 x 10-mm 2 cross-sectional area) and 100 cylindrically-shaped specimens (12.7-mm diameter x 19.0-mm height) for each liner/resin combination were used for the tensile and deformation tests, respectively. Specimen shape and liner thickness were standardized. Specimens were divided into 9 test groups (n=10) and were thermal cycled for 200, 500, 1000, 1500, 2000, 2500, 3000, 3500, and 4000 cycles. Control specimens (n=10) were stored for 24 hours in water at 37 degrees C. Mean bond strength, expressed as stress at failure (MPa), was determined with a tensile test using a universal testing machine at a crosshead speed of 5 mm/min. Analysis of failure mode, expressed as a percent (%), was recorded as either cohesive, adhesive, or both, after observation. Permanent deformation, expressed as a percent (%), was determined using ADA specification no. 18. Data from both tests were examined with a 2-way analysis of variance and a Tukey test (alpha=.05). RESULTS: For the tensile test, Softliner specimens submitted to different thermal cycling regimens demonstrated no significantly different bond strength values from the control; however, there was a significant difference between the PermaSoft control group (0.47 +/- 0.09 MPa [mean +/- SD]) and the 500 cycle group (0.46 +/- 0.07 MPa) compared to the 4000 cycle group (0.70 +/- 0.20 MPa) ( P <.05). With regard to failure type, the Softliner groups presented adhesive failure (100%) regardless of specimen treatment. PermaSoft groups presented adhesive (53%), cohesive (12%), or a combined mode of failure (35%). For the deformation test, there was no significant difference among the Softliner specimens. However, a significant difference was observed between control and PermaSoft specimens after 1500 or more cycles (1.88% +/- 0.24%) ( P <.05). CONCLUSIONS: This in vitro study indicated that bond strength and permanent deformation of the 2 resilient denture liners tested varied according to their chemical composition.

Acrylic Resins↗

PubMed2002

Effect of thermocycling on bond strength and elasticity of 4 long-term soft denture liners.

STATEMENT OF PROBLEM: Two problems found in prostheses with soft liners are bond failure to the acrylic resin base and loss of elasticity due to material aging. PURPOSE: This in vitro study evaluated the effect of thermocycling on the bond strength and elasticity of 4 long-term soft denture liners to acrylic resin bases. MATERIAL AND METHODS: Four soft lining materials (Molloplast-B, Flexor, Permasoft, and Pro Tech) and 2 acrylic resins (Classico and Lucitone 199) were processed for testing according to manufacturers' instructions. Twenty rectangular specimens (10 x 10-mm(2) cross-sectional area) and twenty cylinder specimens (12.7-mm diameter x 19.0-mm height) for each liner/resin combination were used for the tensile and deformation tests, respectively. Specimen shape and liner thickness were standardized. Samples were divided into a test group that was thermocycled 3000 times and a control group that was stored for 24 hours in water at 37 degrees C. Mean bond strength, expressed in megapascals (MPa), was determined in the tensile test with the use of a universal testing machine at a crosshead speed of 5 mm/min. Elasticity, expressed as percent of permanent deformation, was calculated with an instrument for measuring permanent deformation described in ADA/ANSI specification 18. Data from both tests were examined with 1-way analysis of variance and a Tukey test, with calculation of a Scheffé interval at a 95% confidence level. RESULTS: In the tensile test under control conditions, Molloplast-B (1.51 +/- 0.28 MPa [mean +/- SD]) and Pro Tech (1.44 +/- 0.27 MPa) liners had higher bond strength values than the others (P <.05). With regard to the permanent deformation test, the lowest values were observed for Molloplast-B (0.48% +/- 0.19%) and Flexor (0.44% +/- 0.14%) (P <.05). Under thermocycling conditions, the highest bond strength occurred with Molloplast-B (1.37 +/- 0.24 MPa) (P <.05). With regard to the deformation test, Flexor (0.46% +/- 0.13%) and Molloplast-B (0.44% +/- 0.17%) liners had lower deformation values than the others (P <.05). CONCLUSION: The results of this in vitro study indicated that bond strength and permanent deformity values of the 4 soft denture liners tested varied according to their chemical composition. These tests are not completely valid for application to dental restorations because the forces they encounter are more closely related to shear and tear. However, the above protocol serves as a good method of investigation to evaluate differences between thermocycled and control groups.

Acrylic Resins↗

PubMedDate not supplied

Dimensional stability of distances between posterior teeth in maxillary complete dentures.

The aim of this study was to assess the displacement of posterior teeth in maxillary complete dentures stored in water at 37 degrees C. Twenty acrylic resin-based maxillary complete dentures were constructed with the anterior teeth arranged in normal overlap and the posterior teeth in Angle class I. Metallic pins were placed on the labial cusp of the first premolars (PM), and on the mesiolabial cusp of the second molars (M). The final acrylic resin pressing was made in a metallic flask with aid of the RS tension system, and polymerized in a moist-hot cycle at 74 degrees C for 9 hours. The dentures were deflasked after cooling in their own polymerizing water or after cooling in polymerizing water plus bench storage for 3 hours, and stored in water at 37 degrees C for periods of 7, 30, and 90 days. Following deflasking and after each storage period tested, the PM-PM (premolar to premolar), M-M (molar to molar), LPM-LM (left premolar to left molar), and RPM-RM (right premolar to right molar) distances were measured with an STM Olympus microscope, with an accuracy of 0.0005 mm. Collected data were submitted to ANOVA and Tukey's test (5%). There was no statistically significant difference for the PM-PM, M-M, and LPM-LM distances after all storage periods when the flask cooling methods were considered. With exception of the RPM-RM distance after the 30-days water plus bench storage period, the other distances remained statistically stable.

Acrylic Resins↗