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R K Jayanty

Publications and source records attributed to R K Jayanty.

10 recordsLinked to original sources

Interlaboratory study of a test method measuring total volatile organic compound content of consumer products.

Consumer products are potentially significant sources of volatile organic compounds (VOCs), which are precursors to the formation of ozone in photochemical smog. To address the problem of ozone formation in ambient air, the U.S. Environmental Protection Agency (EPA) has been involved in the development of test methods for measuring the VOC content of consumer products. This paper describes results of an interlaboratory study to estimate the repeatability (precision of analyses performed by a single laboratory) and reproducibility (precision of analyses performed by different laboratories) of the consumer products' VOC measurement method based on EPA Method 24 (for VOCs in surface coatings). The mean method repeatability was 2.7 wt% VOC, and the mean method reproducibility was 4.8 wt% VOC. Method repeatability ranged from 0.2 to 4.4 wt% VOC, and reproducibility ranged from 0.6 to 11.9 weight percent VOC. The precision of the VOC method for consumer products is similar to the precision of EPA Method 24 for surface coatings.

Household Products↗

Validation of a test method for the measurement of methanol emissions from stationary sources.

Title III of the 1990 Clean Air Act Amendments designated methanol as a pollutant to be regulated. The U.S. Environmental Protection Agency (EPA), through a contract with Research Triangle Institute, has developed a method for measuring methanol emissions from stationary sources. The methanol sampling train (MST) consists of a glass-lined heated probe, two condensate knockout traps, and three sorbent cartridges packed with Anasorb 747. Samples are desorbed with a 1:1 mixture of carbon disulfide (CS2) and N,N-dimethylformamide (DMF). Condensate water and CS2/ DMF samples are analyzed by gas chromatography with flame ionization detection. The MST has a practical quantitation limit of approximately 3 ppm for a 20-L sample. Samples were shown to be stable for at least two weeks after collection. Field tests of the MST and the National Council of the Paper Industry for Air and Stream Improvement (NCASI) methanol sampling method were conducted at two pulp and paper mills. Sampling and analysis procedures followed EPA Method 301 requirements. The sampling location for the first field test was the inlet vent to a softwood bleach plant scrubber, where the methanol concentration was approximately 30 ppm. The mean recovery of spike was 108.3% for the MST method and 81.6% for the NCASI method. Although neither method showed significant bias at the 95% confidence level, the between-methods bias was significantly different. A second field test was conducted at a vent from a black liquor oxidation tank where the methanol concentration was approximately 350 ppm. Mean spike recoveries were 96.6 and 94.2% for the MST and NCASI methods, respectively. The biases of the two methods and the between-methods bias were not significantly different for the second field test.

Air Pollutants↗

Summary of the 1992 EPA/A&WMA International Symposium: measurement of toxic and related air pollutants.

A joint conference cosponsored for the seventh year by the Atmospheric Research and Exposure Assessment Laboratory (AREAL) of the U.S. Environmental Protection Agency (EPA) and the Air & Waste Management Association (A&WMA) was held in Durham, North Carolina, May 4-8, 1992. The technical program consisted of 200 presentations held in 23 technical sessions and covered recent advances in ambient and source measurement techniques for air pollutants. The symposium was attended by almost a thousand professionals from the United States and other countries, covered a wide range of measurement topics, and was supported by 90 exhibitors of instrumentation and consulting services. This overview highlights the technical presentations of the symposium.

Air Pollutants↗

Evaluation of canisters for measuring emissions of volatile organic air pollutants from hazardous waste incineration.

Regulation to control air emissions of toxic organic compounds require the collection and analysis of effluent gas from low level sources such as hazardous waste incinerators. The standard SW-846 Method specifies the use of Tenax and Tenax/charcoal adsorbent traps for collection of volatile organics from incinerators. This study evaluates passivated stainless steel canisters as an alternative to adsorbent traps to eliminate some of the problems associated with adsorbent sampling. Initially the stability of 18 nonpolar, volatile organic compounds was determined in Summa-treated stainless steel canisters with greater than 100 ppmv HCl and saturated with water vapor. All 18 components were stable for a two-week period; however, an interference caused a 10-fold increase in the FID response of trichloroethylene, toluene, and chlorobenzene. No interference of the ECD response was found for any of the 11 compounds detected with the ECD including trichloroethylene. A pilot scale incinerator was sampled using canisters, and the destruction efficiency of 1,1,1-trichloroethane was determined at a concentration of less than 0.5 ppbv while determining 1,1-dichloroethylene, the major product of incomplete combustion, at a concentration of 8000 ppbv from the same sample.

Air Pollutants, Occupational↗

Summary of the 1989 EPA/A&WMA International symposium: measurement of toxic and related air pollutants.

A joint conference, for the fourth straight year cosponsored by the Air & Waste Management Association's TP-6, TP-7, and ITF-2 technical committees, and the Atmospheric Research and Exposure Assessment Laboratory of the U.S. Environmental Protection Agency, was held at Raleigh, North Carolina, May 2-5, 1989. The technical program consisted of 145 presentations, held in 14 separate technical sessions, on recent advances in the measurement and monitoring of toxic and related pollutants found in ambient and source atmospheres. Covering a wide range of measurement topics and superbly supported by 57 exhibitors of instrumentation and consulting services, the symposium was enthusiastically received by more than 700 attendees from the United States and other countries. This overview contains a selection of the highlights from the technical presentations. A synopsis of the keynote address to the symposium is also included.

Air Pollutants↗