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R Melgar

Publications and source records attributed to R Melgar.

4 recordsLinked to original sources

Vermicomposting of a lignocellulosic waste from olive oil industry: a pilot scale study.

The vermicomposting with Eisenia andrei of dry olive cake, a lignocellulosic waste produced during the extraction of olive oil, either alone or mixed with municipal biosolids, was studied in a nine-month pilot scale experiment. Number and biomass of earthworms and enzyme activities were periodically monitored and relevant properties of the final products were determined. In the assayed substrates, the total biomass of earthworms increased at the end of the experimental period between 9 and 12-fold respectively in comparison with the earthworm biomass initially inoculated. The increase in hydrolytic enzymes and overall microbial activity during the vermicomposting process indicated the biodegradation of the olive cake and resulted in the disappearance of the initial phytotoxicity of the substrate. However, the recalcitrant lignocellulosic nature of the dry olive cake prevented suitable humification during the vermicomposting process. For this reason, in addition to organic amendments, other management procedures should be considered.

Animals↗

A novel GC/MS derivatization method for amphetamines.

Many widely used methods for derivatizing drugs of the amphetamine group for GC/MS are problematic. The difficulties with these methods include incompatibility with other derivatizing agents, short column life, lack of abundant high molecular weight ions, and the potential for interference from other drugs. The present procedure is an effort to reduce some of these problems by the use of a novel derivatizing agent, N-methyl-N-t-butyldimethylsilyl trifluoroacetamide (MTBSTFA). We describe here an MTBSTFA derivatization method for amphetamine (AMP) and methamphetamine (MAMP) that leads to stable derivatives that are well-separated from potential interferences and features high molecular weight fragments suitable for selected ion monitoring. The procedure is linear to approximately 3000 ng/mL for both AMP and MAMP and appears to be both precise and sensitive. Furthermore, it seems to have no adverse effect on column life.

Acetamides↗