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S J Smolenski

Publications and source records attributed to S J Smolenski.

13 recordsLinked to original sources

Reversed-phase high-pressure liquid chromatography of some tryptamine derivatives.

A quantitative reversed-phase high-pressure liquid chromatographic method is described for tryptamine, bufotenine, N-methyltryptamine and N,N-dimethyl tryptamine. All compounds were eluted with base-line separation within 15 min. The method is used to determine the tryptamine level in a leaf extract of Acacia podalyriaefolia A. Cunn. Satisfactory recoveries of tryptamine from plant material, and N,N-dimethyltryptamine from urine were obtained.

Bufotenin↗

Isolation and identification of three new flavones from Achillea millefolium L.

Column chromatography on silica gel of a petroleum ether extract of the flowering heads of Achillea millefolium L. allowed three flavones to be separated and identified. Spectral studies (PMR, mass spectrometry, and UV) and a comparison with data for compounds reported in the literature established the flavones as 5-hydroxy-3,6,7,4'-tetramethoxyflavone, artemetin, and casticin. These compounds have not been reported previously as constituents of A. millefolium.

Flavonoids↗

Alkaloid screening. VI.

One thousand and five plant extracts were screened for the presence of alkaloids. The number of positive tests obtained was 267, or 34.01%. New to the literature are 137 species. In the five previous communications (1-5) in this series we have reported on the screening of 4,990 plant extracts for alkaloids. These 4,990 extracts represented 4,103 species of plants, of which 1,069 gave positive tests.

Alkaloids↗

Akaloid screening. VII.

One thousand and five plant extracts were screened for the presence of alkaloids. The number of positive tests obtained was 190, or 18.91%. There were 153 species found to contain alkaloids that are new to the literature. In the six previous communications (1-6) we have reported on the screening of 5,995 plant extracts for alkaloids. These extracts represented 4,888 species of plants, of which 1,336 gave positive alkaloid tests.

Alkaloids↗

Alkaloid screening. VIII.

One thousand plant extracts were screened for the presence of alkaloids. The number of positive tests was 185 (18.5%). There are 107 new alkaloid-containing species.

Alkaloids↗