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Biomedical subjects

S S Khajotia

Publications and source records attributed to S S Khajotia.

8 recordsLinked to original sources
PubMed2001

The effect of saliva on shear bond strengths of hydrophilic bonding systems.

Failure of orthodontic bonded attachments and brackets is mostly attributed to contamination of the enamel surface. To overcome this problem, materials have been developed that purportedly overcome the moisture and contaminants present in the oral environment. This study compared the shear bond strengths of 2 lightcured hydrophilic bonding systems, Transbond XT with MIP (3M/Unitek, Monrovia, Calif) and Assure (Reliance Orthodontics, Itasca, Ill) with a hydrophobic bonding system, Transbond XT with XT primer (3M/Unitek). Comparison tests were conducted under 4 enamel surface conditions: (1) etched and dried; (2) etched and moistened with artificial saliva; (3) etched, primed, and moistened with artificial saliva; and (4) etched, primed, moistened with artificial saliva, and reprimed. In addition, an adhesive remnant index score was used to determine the amount of adhesive remaining on the tooth. Stainless steel brackets with mesh-backed pads (n = 144) were bonded to bovine teeth. Bond strength was then tested in shear using an Instron mechanical testing instrument. There were significant differences in the bond strengths among the products (P <.05), within surface treatments (P <.05), and among the different bonding materials in combination with various surface treatments (P <.05). Treatments 1 and 4 showed the highest mean bond strengths adhesive remnant index scores, whereas treatments 2 and 3 showed the lowest mean bond strengths and scores.

Acid Etching, Dental↗
PubMed2000

Fluoride concentrations in bottled water.

Bottled water use and lack of adequate labeling have given rise to questions regarding fluoride intake. This study examined fluoride concentration of commercially available bottled water products, determined if significant differences existed among the products, and explored packaging date as a variable on the concentration of fluoride. The values were compared to the ADA guideline for optimally fluoridated water and the American Academy of Pediatric Dentistry recommended schedule for fluoride supplementation. Five commercial brands were chosen for the study. Three bottles of each brand, each with different batch dates, were purchased. Following calibration, six tests were conducted on each bottle using the Hach DR-100 Colorimeter System for fluoride analysis and the values were recorded. Data were analyzed using a two-tailed ANOVA and Tukey's HSD Test (p = 0.05). The results showed that significant differences in fluoride concentrations existed among the five brands. For three brands, significant differences existed between the batches. All products had fluoride concentrations that fell below the ADA accepted standards for optimally fluoridated water. Due to the significant variability in fluoride concentration between products and batches, dental providers should advise their patients that bottled water might not contain optimal levels of fluoride.

Analysis of Variance↗
PubMed1999

Elimination, via high-rate laser dilatometry, of structural relaxation during thermal expansion measurement of dental porcelains.

OBJECTIVES: Thermal expansion measurement of glassy materials is complicated by thermal history effects. Excess volume--trapped in quenched dental porcelains after firing--collapses via structural relaxation on first slow heating during conventional dilatometry, making the thermal expansion coefficient (alpha) obtained on first heating unreliable. The purpose of this study was to determine whether porcelain thermal expansion measurement at high thermal rates could minimize the influence of thermal history. METHODS: Eight thermal expansion specimens each of six body porcelains and the Component No. 1 (leucite-containing) frit prepared according to the patent by Weinstein et al. (US Patent No. 3,052,982) were subjected to three heat-cool conventional dilatometry runs at 3 degrees C/min, while eight thermal expansion specimens of each porcelain were reserved as untreated controls. Eight hollow, cylindrical specimens of the same brands were subjected to three heat-cool laser dilatometer thermal expansion runs at 600 degrees C/min, while eight cylindrical specimens of each porcelain were reserved as untreated controls. Thermal expansion data (25-500 degrees C) of all specimens were subjected to repeated measures analysis of variance. RESULTS: The alpha obtained on first slow heating was significantly lower than values for succeeding slow heat and cool runs in all porcelains (P < 0.001). High-rate alpha obtained on first heating was not significantly different from values of succeeding heat and cool runs in all porcelains (P > 0.05). SIGNIFICANCE: Conventional dilatometer measurements demonstrated occurrence of structural relaxation, as evidenced by the significant difference in the first heating and subsequent runs. High-rate laser dilatometry eliminated structural relaxation, thereby providing a thermal expansion measurement that is free of interference from thermal history effects.

Analysis of Variance↗
PubMed1999

Effect of toothbrushing on elemental release from dental casting alloys.

PURPOSE: This study assessed the effect of toothbrushing on the elemental release from common dental casting alloys. MATERIALS AND METHODS: A Au-Pt high-noble alloy, a Au-Pd high-noble alloy, a Pd-Cu-Ga noble alloy, and a Ni-Cr base-metal alloy were placed into a biological medium for 1 week to allow equilibration of elemental release, then brushed for 30 minutes at 90 strokes/min under 200 g of force with a soft toothbrush. The brushing was performed in neutral saline or lactic acid at pH 4 with or without toothpaste. The alloys were then transferred back into a biological medium for 1 week. Atomic absorption spectroscopy was used to measure the mass lost from each alloy during and in the week after brushing. Mass loss was expressed as micrograms per square centimeter of alloy surface, and the various brushing conditions were compared by analysis of variance and Tukey multiple comparison intervals (alpha = 0.05). RESULTS: During brushing, element release increased significantly over nonbrushed controls for all alloys except the Ni-Cr. Toothpastes, acidic solutions, or combinations of these conditions with toothbrushing further enhanced elemental release, but Ni release from the Ni-Cr alloy increased the most (30-fold). In the week after brushing, brushing alone increased elemental release only from the Ni-Cr alloy. However, toothpastes and acidic solutions increased elemental release for all alloys significantly, except for the Au-Pd alloy. In general, elemental release during brushing was far greater than in the week after brushing. CONCLUSIONS: Under the conditions of this study, toothbrushing increased the elemental release from dental casting alloys.

Analysis of Variance↗
PubMed1998

Effect of pH on element release from dental casting alloys.

STATEMENT OF PROBLEM: Dental casting alloys are subjected to transient acidity in the oral environment, yet most studies have not investigated the effects of these transient environments on elemental release from alloys. Elemental release is important because it plays a significant role in alloy biocompatibility. PURPOSE: It was hypothesized that acidic environments would increase elemental release from dental alloys during exposure and after the acidic environment was removed. This hypothesis was based on the known increase in release of nickel from nickel-based alloys in an acidic environment. MATERIAL AND METHODS: High-noble, noble, and base metal casting alloys were exposed for 30 minutes to solutions with pH ranging from 1 to 7. Elemental release of representative elements was measured by means of atomic absorption spectrometry during the exposure and in the week after the exposure. This release was compared with elemental release in the week before the exposure. RESULTS: High-noble and noble alloys were resistant to acidic environments. A pH of 4 did not increase elemental release during or after exposure. A pH 1 environment slightly elevated release of Ag, Cu, and Pd in some alloys. However, a Ni-based alloy released large amounts of Ni during the acidic exposure of pH 1 or 4, and more importantly, in the week after the exposure as well. Increased time of exposure to acid did not alter elemental release from noble or high-noble alloys, but markedly increased release from the Ni-based alloy. CONCLUSIONS: Transient exposure of casting alloys to an acidic oral environment is likely to significantly increase elemental release from Ni-based alloys, but not from high-noble or noble alloys.

Analysis of Variance↗
PubMed1997

Fracture toughness and load relaxation of dentin bonding resin systems.

OBJECTIVES: The fracture toughness (KIC) and load relaxation of four dentin bonding resins were determined to characterize some of the mechanical properties of these materials after polymerization. METHODS: A total of 40 single-edge notch bar specimens were fabricated, 10 each of four commercially available brands, and subjected to three-point bending until fracture, as described in ASTM Standard E399-83 (1991a). The critical stress intensification factor, KIC, was derived for each specimen and compared by analysis of variance and Scheffé's multiple comparisons test (p < 0.01). To study the load relaxation characteristics, five rectangular specimens (without notches) of each brand were subjected to three-point loading until a predetermined limiting load value was reached. The test load was allowed to relax for 4 min, after which the specimen was unloaded to the zero load condition, and the load was allowed to build up on its own accord for 3 min. Load relaxation values were measured from the chart, and the mean percent load drop was calculated. The load relaxation data were compared using analysis of variance and Scheffé's multiple comparisons test (p < 0.05). RESULTS: The fracture toughness (KIC) values of the four adhesive resins studied in this investigation ranged from 0.37-0.94 MPa.m0.5 and were statistically different from each other (p < 0.001). The load relaxation values were found to be greatest within the first 0.5 min, with the total load relaxation of the four bonding agents ranging from 16%-30%. Two of the materials studied showed significantly different short-term load relaxation behavior than the other two resins (p < 0.05). SIGNIFICANCE: Bonding agents can be implicated as one of the factors that weaken the interface between the dentin and the composite restorative material. These materials are capable of a rapid short-term response, demonstrating significant load relaxation in the first 0.5 min after loading.

Acrylates↗
PubMed1996

Potential interference of leucite crystallization during porcelain thermal expansion measurement.

OBJECTIVES: The elevated temperatures and slow heating and cooling rates associated with a thermal expansion run provide a thermal treatment comparable to those previously shown to produce leucite crystallization in dental PFM porcelains. The purpose of this study was to determine whether the exposure of dental porcelains to the time-temperature profile of a thermal expansion run could result in leucite crystallization, a potential interference with the accurate determination of the thermal expansion coefficient. METHODS: A total of 112 thermal expansion specimens were prepared, 16 each of six commercially available body porcelains, as well as the "Component No. 1" (leucite-containing) frit of the Weinstein et al. (1962) patent. In a randomized design, the leucite contents of specimens subjected to a 3 degrees C/min thermal expansion run were compared to those of untreated controls. The leucite content of each specimen was determined via quantitative X-ray powder diffraction using an Al2O3 internal standard. One-tailed t-tests were applied to determine whether the dilatometer thermal treatment produced a statistically significant increase in leucite content. RESULTS: The heat treatment afforded by a 3 degrees C/min dilatometer run was not sufficient to induce measurable leucite crystallization in any of the porcelains examined in this study. SIGNIFICANCE: The crystallization of leucite during a dilatometer heating run can be ruled out as a possible interference with the determination of the coefficient of thermal expansion of dental porcelain.

Aluminum Silicates↗