PubMed Health⌕ Search

Biomedical subjects

Susumu Arimori

Publications and source records attributed to Susumu Arimori.

5 recordsLinked to original sources

Simple protocol for NMR analysis of the enantiomeric purity of diols.

[reaction: see text] A practically simple three-component chiral derivatization protocol for determining the enantiopurity of chiral 1,2-, 1,3-, and 1,4-diols by (1)H NMR spectroscopic analysis is described. The method involves treatment with 2-formylphenylboronic acid and enantiopure alpha-methylbenzylamine to afford a mixture of diastereoisomeric iminoboronate esters whose ratio is an accurate reflection of the enantiopurity of the parent diol.

Journal Article↗