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T B Whitaker

Publications and source records attributed to T B Whitaker.

9 recordsLinked to original sources

On testing normality using several samples: an analysis of peanut aflatoxin data.

Eight samples of size 16 and three samples of size 15 consisting of replicate determinations of aflatoxin in peanut subsamples were considered. These data were analyzed to decide whether the samples could have arisen from two-parameter normal or lognormal parents. The method of analysis consisted of first transforming the individual samples in such a way that the transformed values had uniform distributions on the unit interval under the null hypothesis. The transformed values were then pooled and tested for uniformity. Results of the analysis indicated that the normal model fitted the data quite well and definitely better than the lognormal model.

Aflatoxins

Simulation of aflatoxin testing plans for shelled peanuts in the United States and in the export market.

The 1987 United States aflatoxin testing plan for shelled peanuts was designed with a final accept level of 25 parts per billion (ppb) total aflatoxin. Some of the importers of U.S. peanuts use aflatoxin testing plans with accept levels lower than 25 ppb. For example, the accept level of a testing plan used in The Netherlands is 5 ppb B1 or 10 ppb total aflatoxin. Whenever export lots are re-tested for aflatoxin by an importing country, some lots accepted in the United States will be rejected by the importing country's aflatoxin testing plan. Computer models were developed to determine the effects of decreasing the final accept level of the U.S. testing plan on the number of lots accepted and rejected in the United States and the number of exported lots accepted and rejected by The Netherlands testing plan. Decreasing the final accept level of the U.S. testing plan from 25 to 5 ppb increased the number of lots rejected in the United States by 371% while reducing the number of exported lots rejected by 51%. For every additional 8.3 lots rejected in the United States, one less export lot will be rejected.

Aflatoxins

Optimum methanol concentration and solvent/peanut ratio for extraction of aflatoxin from raw peanuts by modified AOAC method II.

The amount of aflatoxin extracted from raw peanuts by using the water-slurry modification of AOAC Method II was determined for 49 different combinations of methanol concentrations and solvent/peanut ratio. Results indicate that the amount of aflatoxins B1 and B2 extracted from raw peanuts is a function of both methanol concentration and solvent/peanut ratio, and a cubic equation was developed, using regression techniques, to describe the combined effects. From the functional relationship, the predicted methanol concentration and solvent/peanut ratio that extracts the most aflatoxin B1 was computed to be 60.0% and 10.8 mL solvent/g peanuts, respectively. This combination extracted 12.1% more aflatoxin than did AOAC Method II.

Aflatoxins