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PubMed · 1365712

Two-dimensional J-resolved and SUPERCOSY NMR experiments in the solid state.

W Kolodziejski·J Klinowski
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Abstract

Two 2D experiments, novel to solid-state NMR, are demonstrated using the trimethylsilyl ester of cubic octameric silicate (Q8M8). J-Resolved 13C NMR with BLEW-12 proton homonuclear decoupling reveals the scalar 13C-1H couplings and 29Si SUPERCOSY the connectivities of silicon atoms in the distorted Q8 cube.

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CarbonCarbon IsotopesHydrogenIsotopesMagnetic Resonance SpectroscopyMolecular StructureSilicatesSiliconJournal ArticleResearch Support, Non-U.S. Gov't

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W Kolodziejski, J Klinowski. 1992. Two-dimensional J-resolved and SUPERCOSY NMR experiments in the solid state.. https://doi.org/10.1016/0926-2040(92)90008-w

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