PubMed · 13669467
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V KESZTELE. 1959-05-23. [Cervical lymph node tuberculosis].. https://pubmed.ncbi.nlm.nih.gov/13669467/
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The coupling reactions of cyclic sulfides with a silylated pyrimidine nucleobase using a hypervalent iodine reagent were investigated. The reaction of silylated uracil with cyclic sulfide 12 using PhI=O gave the desired beta-anomer 14 in moderate yield. 4'-Thiouridine (22) was obtained by deprotection of 14.
To cultivate iodine-enriched forest vegetables in the mountainous regions of northeast China, a series of iodine application experiments were conducted. Iodine fertilizer (potassium iodide, KI) was added to the forest soils supporting a variety of wild-vegetable plants, with a dosage gradient of 1.00, 3.33, 10.00, 16.67 and 50.00 mg.kg-1. The results showed that iodine application was an effective approach to obtain iodine-rich vegetable materials, and the iodine contents in treated plants could be 2-40 times higher than control. But, the residual of added iodine in soil was generally not high, only occupying 40%-5% of the application dosage. The accumulation of iodine in plants did not consistently increase with the dosage, which tended to slow down when the application amount increased to 10.00 mg.kg-1. In a comprehensive consideration of soil iodine residual, plant iodine accumulation and application cost, the proper iodine dosage should be approximately 10 mg.kg-1. Soil conditions had significant influence on the efficiency of iodine application, and the cultivated lands should be chosen at fine-textured, fertile, and upper-sloped sites, while sandy soils and down-sloped sites were unfavorable to the preservation of added iodine and to plant absorption.
The structure and rheological properties of water-soluble polysaccharides from industrialized mango pulp were investigated. Soluble fraction (SF) 2 was heterogeneous on high performance size exclusion chromatography, giving two peaks as determined by multi-angle laser light scattering and refractive index detectors. The presence of starch in SF2 was demonstrated by a positive iodine reaction and by 13C nuclear magnetic resonance (NMR) spectroscopy. The presence of pectic polysaccharides was shown by a calorimetric method, 13C-NMR spectroscopy and carboxyl reduction. The main pectic polysaccharide was polygalacturonic acid; type I rhamnogalacturonan was also detected. Analysis of the rheological properties of SF2 showed a pseudoplastic behavior up to 3 g x l(-1). 'Creep and recovery' tests and analysis performed under a dynamic state revealed a weak gel character for solutions at concentrations of 15, 20 and 30 g x l(-1).