PubMed · 292043
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M A de Araújo, J R Rodrigues. 1978. [Amalgam corrosion].. https://pubmed.ncbi.nlm.nih.gov/292043/
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Discoloring and layers on bands and restorations during fixed orthodontic therapy are well known clinical phenomenon. Because of the complexity of etiological factors an in-vitro model was used in this study. Aim of the study was to examine the amounts and sort of metals which are dissolved. Therefore, respectively 25 normed MOD-cavities in Frasaco-teeth were filled with a non-gamma-2-amalgam (Amalcap plus, Vivadent) and condensed manually or mechanically. In addition, ten crowns of a high golden (Maingold SG, Heraeus) as well as a palladium basis alloy (Albabond A, Heraeus) were casted. Then they were banded with stainless steel bands (Dentaurum) and cemented with a glass ionomer cement (Ketac Cem, Espe). The probes were given into a 0.1 molar lactic acid for seven days at 37 degrees C. Using ICP (ion coupled plasma) analysis the corrosion solution was examined for elements. High levels of Zn- and Al-ion contents were found, which are components of the used cements. The filling materials themselves mainly set free small amounts of Ag, Sn or Cu. The steel band released Fe, Cr, Ni and Ti. The combination of filling material and band resulted in a higher release of most ions.
Microcracks, flaws, and voids inside a metal-porcelain restoration may cause the restoration to fracture in service. Such cracks result in the concentration of stresses. The dynamic nature of the stresses due to mastication promotes crack growth. In addition, corrosive components of the oral environment enhance the growth rate. In the present investigation, fracture mechanics has been used to analyze the in vitro resistance to fracture of the porcelain-fused-to-metal restoration. The risk of a clinical failure of porcelain-fused-to-metal decreases with enlarged crack resistance (increasing work of fracture). The work of fracture represents an average of the energy for initiation and propagation of a crack through the interface separating porcelain and metal. This work also indicates a material's ability to stop a crack once it is moving. This study utilized the three-point bending test for the crack resistance measurement, and investigated one palladium and five base metal alloys. Corrosive components of the oral environment and the details of firing were of crucial importance for long-term bond stability.
A number of important reactions occur in clinical amalgam restorations. This investigation examined the extent of the gamma-1 to beta-1 transformation in a variety of amalgam restorations retrieved from clinical trials. Sixteen restorations of five brands of low Cu amalgams, 28 restorations of four brands of high Cu blended amalgams, and eight restorations of three brands of high Cu single particle amalgams were studied. The extent of the gamma-1 to beta-1 transformation was determined by the ratio of the integrated intensity of the 002 beta-1 peak to the 330 gamma-1 peak in x-ray diffraction patterns. These values were correlated with age, marginal deterioration grade, and residual Hg content. Restorations consistently contained more beta-1 than comparable laboratory controls. Blended high Cu amalgams generally contained more beta-1, which was correlated with better marginal grades. Beta-1 content was inversely related to residual Hg content. No other associations could be established. A model of the complex interactions between corrosion and transformations was developed.