PubMed · 8835857
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R F Harris. 1996-07-01. Gender bender.. https://doi.org/10.1016/s0960-9822(02)00586-9
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An efficient approach to synthesize delta 6-estrogens is described. The key steps in the synthesis are the introduction of a hydroxyl group at the C-6 position of a suitably protected estrogen using a superbase and subsequent dehydration with Martin sulfurane reagent or methyltriphenoxyphosphonium iodide. The two-step synthetic procedure readily gave the delta 6-estrogens in high yield.