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Gas chromatography and electron capture detection of benzophenones. Part XI. Applications in the oxidation of gem-diphenylmethane substituted compounds by barium peroxide.

P Hartvig·W Handl
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BariumBenzhydryl CompoundsBenzophenonesChemical PhenomenaChemistryChromatography, GasHydrogen-Ion ConcentrationOxidation-ReductionPeroxidesJournal Article

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P Hartvig, W Handl. 1975. Gas chromatography and electron capture detection of benzophenones. Part XI. Applications in the oxidation of gem-diphenylmethane substituted compounds by barium peroxide.. https://pubmed.ncbi.nlm.nih.gov/889/

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PubMed1978

Preparative-scale enzymic synthesis of D-[14C]ribulose 1,5-bisphosphate.

A procedure is described to prepare uniformly labelled D-[14C]ribulose 1,5-bisphosphate enzymically from uniformly labelled D-[14C]glucose through the coupled reactions catalysed by hexokinase (EC 2.7.1.1), glucose 6-phosphate dehydrogenase (EC 1.1.1.49), 6-phosphogluconate dehydrogenase (EC 1.1.1.44) and 5-phosphoribulokinase (EC 2.7.1.19). All reagents utilized in the method are commercially available. The procedure is a reliable preparative-scale method for synthesizing the dibarium salt of D-[14C]ribulose 1,5-biphosphate with a specific radioactivity up to 7 mCi/mmol and a purity near 90%. The final product was free of other 14C-labelled sugars, sugar phosphate esters, Pi and nucleotides.

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