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PubMed · 9048377

Charge-coupled device-based area detectors.

E M Westbrook·I Naday
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Crystallography, X-RayFiber Optic TechnologyImage EnhancementLuminescent MeasurementsModels, ChemicalJournal ArticleResearch Support, U.S. Gov't, Non-P.H.S.Research Support, U.S. Gov't, P.H.S.

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E M Westbrook, I Naday. 1997. Charge-coupled device-based area detectors.. https://pubmed.ncbi.nlm.nih.gov/9048377/

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Chemistry of re with N,N'-bis(2-pyridylmethyl)ethylenediamine (H2pmen): hydrolysis, dehydrogenation, and ternary complexes.

A number of Re complexes with N,N'-bis(2-pyridylmethyl)ethylenediamine (H2pmen) have been made from [NH4][ReO4]. [ReOCl2(H2pmen)]Cl, [ReOCl(Hpmen)][ReO4], and [ReO2(H2pmen)][ReO4] are related by hydrolysis/HCl substitution. [ReOCl(Hpmen)][ReO4] was structurally characterized and found to contain a water-stable amido-Re bond. Dehydrogenation of the N-donor ligand from each amine to imine with concomitant two-electron reduction of the Re center occurs readily in these systems. With suitable 3-hydroxy-4-pyrones, ternary complexes such as [ReIIICl(ma)(C14H14N4)][ReO4].CH3OH, 5, were made from [NH4][ReO4], H2pmen.4HCl and pyrones in one-pot syntheses. 5, a seven-coordinate ReIII complex, was structurally characterized.

Crystallography, X-Ray↗