PubMed Health⌕ Search

PubMed · 9515439

A single-component bonding system microleakage study.

Abstract

The microleakage of a one-component bonding system is compared to a two-component system and a control. Class V cavity preparations were prepared in extracted teeth under high speed and water coolant so that incisal/occlusal margins were in enamel, and gingival margins were in dentin. Group I was restored with composite and no bonding agent; Group II was restored with Prime and Bond and composite, and Group III was restored with ProBond and composite. All specimens were thermocycled in fuchsin dye to evaluate the degree of microleakage. Significant differences were observed between the no bonding agent group and the Prime and Bond and ProBond groups. The results indicate that the one-step dentin bonding system has the ability to prevent microleakage effectively at both composite-enamel and composite-dentin tooth surface interfaces.

Explore related subjects

Keep this discovery

Explore connections, maps & timelines

BibTeXRIS

L Settembrini, J P Gultz, W Scherer, J Kaim. A single-component bonding system microleakage study.. https://pubmed.ncbi.nlm.nih.gov/9515439/

Cite the original work for its findings. Save a collection to share your selection of sources.

KEEP EXPLORING

Related citations

Determination of double bond conversion in dental resins by near infrared spectroscopy.

OBJECTIVES: This study determined the validity and practicality of near infrared (NIR) spectroscopic techniques for measurement of conversion in dental resins. METHODS: Conversion measurements by NIR and mid-IR were compared using two techniques: (1) The conversion of 3mm thick photopolymerized Bis-GMA/TEGDMA resin specimens was determined by transmission NIR. Specimens were then ground and reanalyzed in KBr pellet form by mid-IR. (2) As further verification, thin resin films were photocured and analyzed by mid-IR. Multiple thin films were then compressed into a thick pellet for examination by NIR. RESULTS: Conversion values obtained by NIR and mid-IR techniques did not differ significantly. A correction for changing specimen thickness due to polymerization shrinkage was applied to NIR conversion measurements since an internal standard reference peak was not employed. Sensitivity of the NIR technique was superior to those based on the mid-IR. SIGNIFICANCE: The nondestructive analysis of conversion in dental resins by NIR offers advantages of convenience, practical specimen dimensions and precision compared with standard mid-IR analytical procedures. Because glass is virtually transparent in the NIR spectrum, this technique has excellent potential for use with filled dental resins as well.

Bisphenol A-Glycidyl Methacrylate↗

Whisker-reinforced dental core buildup composites: effect of filler level on mechanical properties.

The strength and toughness of dental core buildup composites in large stress-bearing restorations need to be improved to reduce the incidence of fracture due to stresses from chewing and clenching. The aims of the present study were to develop novel core buildup composites reinforced with ceramic whiskers, to examine the effect of filler level, and to investigate the reinforcement mechanisms. Silica particles were fused onto the whiskers to facilitate silanization and to roughen the whisker surface for improved retention in the matrix. Filler level was varied from 0 to 70%. Flexural strength, compressive strength, and fracture toughness of the composites were measured. A nano-indentation system was used to measure elastic modulus and hardness. Scanning electron microscopy (SEM) was used to examine the fracture surfaces of specimens. Whisker filler level had significant effects on composite properties. The flexural strength in MPa (mean +/- SD; n = 6) increased from (95+/-15) for the unfilled resin to (193+/- 8) for the composite with 50% filler level, then slightly decreased to (176+/-12) at 70% filler level. The compressive strength increased from (149+/-33) for the unfilled resin to (282+/-48) at 10% filler level, and remained equivalent from 10 to 70% filler level. Both the modulus and hardness increased monotonically with filler level. In conclusion, silica particle-fused ceramic single-crystalline whiskers significantly reinforced dental core buildup composites. The reinforcement mechanisms appeared to be crack deflection and bridging by the whiskers. Whisker filler level had significant effects on the flexural strength, compressive strength, elastic modulus, and hardness of composites.

Bisphenol A-Glycidyl Methacrylate↗

Preparation, morphological characterization, and activity of thin films of horseradish peroxidase.

Active uniform films of horseradish peroxidase (HRP) have been prepared by covalent binding on Si/SiO(2) or glass supports previously activated by silanization and succinylation. Labeling by fluorescent or by Electron Spin Resonance (ESR) probes was used to quantify the surface density of active groups and of horseradish peroxidase. Atomic Force Microscopy (AFM) imaging was used to characterize the surface morphology. We observed that a non-uniform protein adsorption due to physical interactions was present when the supports were not activated for covalent binding and was, in large part, removed by washing. The enzyme deposited by covalent binding formed homogeneous layers with a height in the range 60-90 A. By using a fluorescent label, we calculated a protein density of 3.6 x 10(12) molecules cm(-2) on Si/SiO(2), corresponding to an estimated area per molecule of 2800 A(2) which is in agreement with the value expected on the basis of the crystallographic data considering the formation of a monomolecular layer. The protein density of the layer immobilized on glass was similar (1.9 x10(12) molecules cm(-2)). The enzyme immobilized on both supports showed a k(cat)/K(M) being of the order of 3-5x10(5) M(-1)s(-1) that is 1/20th of free HRP. The half-life time of the activity of the enzyme immobilized by covalent binding was longer than 40 days at 6 degrees C.

Bisphenol A-Glycidyl Methacrylate↗