Repeatability and reproducibility estimates from collaborative studies based on total concentration of trace analytes.

F D McClure

PubMed · 9680704

Repeatability and reproducibility estimates from collaborative studies based on total concentration of trace analytes.

Abstract

In the process of validating a given analytical method for the total concentration of a trace analyte, the precision indicators, repeatability and reproducibility, are obtained from a collaborative study of the method based on a standard one-way completely randomized model. This report discusses the shortcomings of the statistical models used in such studies, defines the component makeup for estimates of the repeatability and reproducibility variances based on these models, and considers suggestions offered as new policy regarding method performance based on total concentration.

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Aflatoxins Algorithms Carcinogens Food Analysis Microchemistry Models, Statistical Quality Control Reproducibility of Results Journal Article

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F D McClure. Repeatability and reproducibility estimates from collaborative studies based on total concentration of trace analytes.. https://pubmed.ncbi.nlm.nih.gov/9680704/

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