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PubMed2006

Influence of polymerization method, curing process, and length of time of storage in water on the residual methyl methacrylate content in dental acrylic resins.

This study compared the influence of different polymerization methods (heat, auto-, and microwave energy), different curing processes (in the case of heat- and autopolymerized specimens), and length of storage of the polymerized specimens in distilled water at 37 degrees C on the residual methyl methacrylate (MMA) content in dental acrylic resin specimens. Residual MMA of 120 resin specimens were measured using high-performance liquid chromatography. For the heat-polymerized resins, the lowest residual MMA content was obtained when they were given a long-term terminal boil and then stored in the distilled water for at least 1 day. For the autopolymerized resins, the lowest residual MMA content was obtained when they were additionally cured in water at 60 degrees C and then stored in the distilled water at least 1 day. For the microwave-polymerized resins, the lowest residual MMA content was obtained when they were stored in the distilled water at least 1 month. The lowest overall residual MMA content was obtained from heat-polymerized specimens that were given a long-term terminal boil cure and then stored in the distilled water at least 1 day. Different polymerization methods and curing processes have different effects on residual MMA content. It is thus shown that storing a dental acrylic resin specimen in distilled water at 37 degrees C is a simple but effective method of reducing its residual MMA content.

Acrylic Resins↗
PubMed1995

The effect of variation in powder particle size on the doughing and manipulation times and some mechanical properties of acrylic resin.

In this study, the hypothesis examined is that differences in polymer particle size affect the doughing and manipulation times and the mechanical properties of the cured product. Six batches of polymers were used varying in particle size from <38 micrometers diameter to > 75 micrometers diameter. A penetration test was undertaken to investigate the influence of polymer particle size on the doughing and manipulation times of acrylic resin. It was demonstrated that the particle size in the range examined influenced the doughing and manipulation times, the smaller particle sizes having shorter times. No significant difference was demonstrated in the impact resistance of surface hardness of acrylic resin specimens constructed from polymers of varying particle size and although there were some significant differences in the transverse (flexural) strength these were small in real terms. Further, the molecular weight of the polymerised product was found to be consistently higher than that of the original powder component.

Acrylic Resins↗
PubMed1997

Fabrication of acrylic resin copings for CeraOne provisional restorations.

A technique is described for fabricating autopolymerizing acrylic resin copings for CeraOne provisional restorations. This method has the advantage of providing a chemical bond rather than only a bond between the mechanical coping and the relined provisional crown, as is the case when using the provisional components supplied by the manufacturer. The technique describes provisionalization at the time of stage II surgery. This type of coping can also be used after a period of soft tissue healing when a healing abutment is employed. The benefits of the procedure include increased patient satisfaction and reduced chair time for repairs.

Acrylic Resins↗
PubMed1997

The effects of surface machining on heat cured acrylic resin and two soft denture base materials: a scanning electron microscope and confocal microscope evaluation.

STATEMENT OF PROBLEM: Rough surfaces promote the adhesion and colonization of denture plaque, therefore it is important to know the character of the surface left by rotary instruments on denture base materials. As a single microscopic technique can introduce artifact, complementary microscope techniques need to be used. PURPOSE: This study investigated the surface characteristics of the machined surfaces of heat-cured acrylic resin, Molloplast B and Novus. MATERIAL AND METHODS: Scanning electron microscopy and confocal microscopy were used to investigate surfaces that had been prepared with appropriate clinical rotary instruments. Thirty samples of each material were prepared with steel and tungsten carbide burs, Molloplast stones, and Arbor bands. An analysis of variance, with the Scheffe multiple comparison of means test, was used to compare average surface roughness of the individual surfaces. RESULTS: The tungsten carbide bur produced a smoother nongrooved surface than the steel bur on acrylic resin. The roughest surfaces were produced on the soft lining materials by the Arbor band and Molloplast stone. CONCLUSIONS: The confocal microscope is a valuable complementary instrument to scanning electron microscopy and provides surface roughness data by using a noncontact method. Each type of rotary instrument produces its own characteristic surface on denture base materials.

Acrylic Resins↗
PubMed1983

An in vitro and in vivo study of the effect of incorporation of chlorhexidine into autopolymerizing acrylic resin plates upon the growth of Candida albicans.

Chlorhexidine acetate was incorporated into autopolymerizing acrylic resin and, after studying its ability to diffuse out in vitro, an investigation was made into the potential of the mixture to treat palatal candidosis in the rat. Chlorhexidine was found to diffuse out of acrylic in fungicidal concentrations for up to three weeks when mixed with the acrylic powder in the proportion of 7.5% (w/w). At this concentration it was found that palatal candidosis as produced by the technique of Shakir et al. was cured or prevented. However, rats fitted with chlorhexidine supplemented plates were found not to take sufficient food during the experimental period to maintain their body weight.

Acrylic Resins↗
PubMed1982

The use of acrylic resin oral prosthesis in radiation therapy of oral cavity and paranasal sinus cancer.

In radiation therapy of cancers of the oral cavity and the paranasal sinuses, the extent to which the tissues of the oral cavity are included in the radiation treatment portals will determine the severity of the oral discomfort during treatment. This will affect the nutritional status of the patients, and may eventually affect the total dose of radiation which the patients can receive for treatment of their cancers. In cooperation with the Maxillofacial Prosthetic Department, an acrylic resin oral prosthesis was developed. This prosthesis is easy to use and can be made for each individual patient within 24 hours. It allows for maximum sparing of the normal tissues in the oral cavity and can be modified for shielding of backscattered electrons from heavy metals in the teeth. We have also found that acrylic resin extensions can be built onto the posterior edge of post-maxillectomy obturators; this extension can be used as a carrier for radioactive sources to deliver radiation to deep seated tumor nodules in the paranasal sinuses.

Acrylic Resins↗
PubMed2001

Reline materials--handle with care? An investigation into the effect of varying the powder/liquid ratio on some properties of auto-polymerising acrylic resin materials.

INTRODUCTION: The fit of the denture base to the alveolar ridge progressively declines with alveolar ridge resorption. Once a denture becomes ill-fitting there are two main treatment options: to construct a new denture or to restore the fit of the existing denture. A denture may be relined as a laboratory procedure or at the chairside in the dental clinic. The chairside reline technique involves the direct application of auto-polymerising acrylic resin materials to the prepared denture base and the material is allowed to polymerise in the patient's mouth. The reline materials are generally supplied as a powder and a liquid. Clinicians and laboratory dental staff do not always follow manufacturers' recommended guidelines and the tendency can be simply to add varying quantities of powder and liquid until the desired consistency is achieved. This method however may have deleterious effects on the properties of the resultant material. MATERIALS AND METHOD: The aim of the study was to investigate the effect of varying the powder/liquid ratio on some properties of three auto-polymerising acrylic resin reline materials. The properties investigated were the flow characteristics in terms of the manipulation and setting time and the hardness. Four powder and liquid ratios were chosen. RESULTS AND CONCLUSIONS: For all the materials studied, a clinically useful lengthening of the manipulation time can be achieved by increasing the amount of liquid added to the powder. However, this is perhaps offset by the fact that it is associated with a corresponding increase in the setting time and resultant increase in clinical chairside time. There were significant differences in surface hardness when the powder/liquid ratio was altered.

Acrylic Resins↗
PubMed2001

Acrylic resins as rate-controlling membranes in novel formulation of a nine-day 17beta-estradiol transdermal delivery system: in vitro and release modifier effect evaluation.

The feasibility of transdermal controlled delivery system of 17beta-estradiol was investigated by conducting in vitro release studies. Several new 17beta-estradiol unilaminate adhesive devices capable of releasing 17beta-estradiol in a controlled fashion over a 24-h, 36-h, 96-h, 104-h, 168-h, and 216-h period have been developed using acrylic resins (Eudragits E100, RSPO, and RLPO) as adhesive and rate-controlling polymers. The in vitro release profiles of 17beta-estradiol from various TDS unilaminate devices were characterized in a new developed dissolution tester vessel (total volume 200 ml), using a new paddle. The release of drug from different formulations was measured by a sensitive high-performance liquid chromatographic (HPLC) method. The release of drug from all prepared adhesive devices seems to obey zero-order kinetics (r > 0.98). The effect of two different plasticizers (acetyltriburyl citrate [ATBC] and triethyl citrate [TEC]) on the release patterns of 17beta-estradiol from TDS formulations was studied, and they were almost identical. The effect of two different release modifiers, propylene glycol (PG) and myristic acid (MA), on the release pattern of 17beta-estradiol from prepared unilaminate devices was evaluated. It was shown that the use of these release modifiers significantly increased the release of 17beta-estradiol from a TDS unilaminate patch. Furthermore, these data clearly demonstrated that the acrylic resins are suitable polymers for the preparation of 17beta-estradiol TDS adhesive devices.

Acrylic Resins↗
PubMed1990

Denture base acrylic resins: friend or foe?

This article reviews the advantages and disadvantages of denture base acrylic resins. Improvements in areas such as strength and speed of cure are discussed. The authors also emphasize the necessity for investigating the effects of factors other than denture base materials on the incidence of troublesome dentures.

Acrylic Resins↗
PubMed1998

Fabrication of an amalgam core using a customized acrylic resin shell.

This article describes a build-up technique that uses a customized acrylic resin shell for restoring endodontically treated molars that are involved in three-unit fixed partial denture design. The shell confines the amalgam without impinging on the periodontium to ensure a proper core foundation, an ideal tooth preparation, and a more predictable final restoration.

Acrylic Resins↗
PubMed2006

Allergy to auto-polymerized acrylic resin in an orthodontic patient.

This article reports on a 60-year-old woman who had an allergic reaction to methylmethacrylate self-curing acrylic resin during orthodontic treatment. A localized hypersensitive reaction appeared on the palate after an orthodontic retainer was placed. Samples of the acrylic were removed and analyzed with gas chromatography to evaluate the residual monomer level. The residual monomer content was between 0.745% and 0.78%, which did not exceed international standards for this material. Patch tests were performed with several methylmethacrylate resin samples and processed with various techniques; they showed positive reactions. Despite the many alternative products available, self-curing acrylic resin remains widely used because of its low cost, ease of use, and diversity of indications. Orthodontists should be aware that allergic reactions can occur.

Acrylic Resins↗