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PubMed1996

Effect of cubic leucite stabilization on the flexural strength of feldspathic dental porcelain.

Previous studies (Mackert and Evans, 1993) have shown that, when feldspathic dental porcelain is cooled, leucite undergoes a transformation from cubic to tetragonal, associated with a 1.2% volume contraction. This contraction leads to the formation of microcracks in and around the crystals and the development of tangential compressive stresses around the crystals. Our aim was to stabilize increasing amounts of the cubic form of leucite in a leucitereinforced dental porcelain, evaluate its effect on the flexural strength, and characterize its microstructure. The hypothesis was that in the absence of crystallographic transformation, the contraction of the leucite crystals would be lower, thereby limiting the formation of microcracks and minimizing the development of tangential compressive stresses around the leucite particles. We prepared 8 porcelain compositions by mixing increasing amounts of either leucite (KAlSi2O6) or pollucite (CsAlSi2O6) with Optec HSP porcelain (Jeneric/Pentron Inc., Wallingford, CT). Porcelain disks were made from each composition (n = 10 per group). X-ray diffraction analyses showed that the amount of stabilized leucite increased with the amount of pollucite added. The microstructure of the specimens containing tetragonal leucite was characterized by twinned leucite crystals, whereas no twinning was observed in the specimens containing cubic leucite. The evaluation of crack deflection showed that significantly less deflection occurred in the specimens containing cubic leucite. The mean biaxial flexural strength for the group corresponding to 22.2 wt% added pollucite, fired at 1038 degrees C, was significantly lower than that for the control group. The group corresponding to 22.2 wt% added leucite fired at 1150 degrees C exhibited a mean biaxial flexural strength significantly higher than that of all other groups that were not significantly different from the control group. Overall, the stabilization of cubic leucite reduced the flexural strength and the number of crack deflections in leucite-reinforced porcelain. Apparently, the development of tangential compressive stresses around the leucite crystals when cooled is responsible for a significant amount of strengthening of feldspathic dental porcelain.

Aluminum Silicates↗
PubMed2006

Metameric effect between dental porcelain and porcelain repairing resin composite.

OBJECTIVES: The objectives were to evaluate the metameric color and hue angle (degrees) changes between dental porcelain and porcelain repairing resin composites. METHODS: Color of three shades (A2, A3, A3.5) of one brand of dental porcelain and three original shades (A2, A3, A3.5) and three combinations (A2-A3, A3-3.5, A2-A3.5) of three brands of porcelain repairing resin composites (ABT, FSP, TCR) were measured relative to the three standard illuminants (D65, A and F2). Specimen was 2mm in thickness, and 1mm of each shade was layered to make combined shades. Color differences (DeltaEab*) between each shade of dental porcelain and repairing resin composites relative to the three illuminants were calculated, and the ratios of color difference (modified metamerism index) by the change of illuminant were calculated. The ratios of hue angle changes were also compared. RESULTS: Differences in modified metamerism index and the ratio of hue angle changes were influenced by the porcelain shade, brand of resin composites and shade of resin composites. In all three brands of resin composites, A3.5 shade showed the smallest values in modified metamerism index regardless of the shade of porcelain. The average ratio of hue angle changes between each porcelain shade and all the shades of each resin composites showed similar trend when illuminant was changed from D65 to F2. SIGNIFICANCE: Metameric effect between dental porcelain and repairing resin composites varied depending on the shade of porcelain, brand of resin composite and the illuminant. Therefore, shade matching between porcelain and repairing resin composite should be performed carefully. This study confirmed that shades should be matched under the light corresponding to that of use.

Analysis of Variance↗
PubMed1986

Glass transition temperatures of dental porcelains at high heating rates.

The glass transition temperature (Tg) of a dental porcelain is a factor in determining the magnitude of residual stresses introduced in a dental porcelain during cooling of a porcelain-fused-to-metal prosthesis. Tg is known to vary with changes in heating or cooling rate. However, available commercial instrumentation does not permit Tg to be obtained at the very high cooling rates commensurate with actual dental laboratory practice. Tg values are reported here for a number of commercial dental porcelains and other materials. These data were obtained by the bending beam technique, employing a special low thermal-mass furnace to permit rapid heating and cooling rates. Measurements were made at rates as high as 600 degrees C/min. Coefficients of determination (r2) for 1/Tg vs. ln (heating rate) were excellent. This relation is consistent with previously reported low rate Tg data obtained by a different technique.

Dental Porcelain↗
PubMed1996

Microcracks in dental porcelain and their behavior during multiple firing.

Dental porcelains rely on the high-thermal-expansion mineral leucite to elevate their bulk thermal expansion to levels compatible with dental PFM alloys. The microcracks that form around these leucite particles when cooled during porcelain manufacture are a potential source of change in bulk porcelain thermal expansion during fabrication of porcelain-fused-to-metal crowns and bridges. The purpose of the present study was to determine whether multiple firings of commercial dental porcelains could produce changes in microcrack density. Specimens of six commercial porcelains and the "Component No. 1" of the Weinstein patent were fabricated and subjected to 1, 2, 4, 8, and 16 firings. The microcrack densities were determined by quantitative stereology, whereby intersections of microcracks were counted with a test grid. The microcrack data were subjected to linear regression analysis and analysis of variance. The microcrack densities of four of the six porcelains and the Component No. 1 frit were not significantly affected by the number of firings (p > 0.05). One porcelain exhibited a weak but highly significant positive correlation between microcrack density and multiple firings (r2 = 0.24, p = 0.0003), while the remaining porcelain exhibited a weak but statistically significant negative correlation between microcrack density and multiple firings (r2 = 0.15, p = 0.006). The results of this study indicate that even for porcelains that exhibit a measurable change in microcrack density as a function of multiple firings, the magnitude of the increase or decrease in microcrack density after several firings is sufficiently small to cause only negligible shifts in porcelain bulk thermal expansion.

Aluminum Silicates↗
PubMed1989

Phase identification in dental porcelains for ceramo-metallic restorations.

Most commercial dental porcelains designed for ceramo-metallic restorations are partially crystallized feldspathic glasses (glass-ceramics) that consist of low (tetragonal) leucite (K2O.Al2O3.4SiO2) crystals embedded in a glassy matrix. In this work, we have identified the crystalline phases in eight commercial dental porcelains (four enamels and four dentin bodies) in both powder (unfired) and sintered forms, by x-ray diffraction, emission spectroscopy analysis, reflection optical microscopy, and scanning electron microscopy. Besides low leucite and glass, we have found a second crystalline phase in the sintered and slow-cooled porcelains that we propose to be potash feldspar (K2O.Al2O3.6SiO2). It was impossible to ascertain whether these synthetic crystals may be sanidine, orthoclase, or microcline. The precipitation of feldspar during cooling is explained in terms of the crystallization behavior of typical body compositions in the ternary-phase diagram K2O-Al2O3-SiO2. Ceramography confirms the martensitic (displacive) nature of the transformation from high (cubic) to low (tetragonal) leucite upon cooling.

Crystallography↗
PubMed1990

Viscosity of dental porcelains in glass transition range.

Changes in the viscosity of dental porcelain as a function of temperature are the controlling factor determining incompatible stresses in porcelain-fused-to-metal restorations. A new method was used to estimate viscosity using a viscoelastic analytical model that considers the relation between the heating rate and deformation temperature (Td) of dental porcelain with stress applied during heating. The activation energy of viscous flow and the viscous constant in the Arrhenius equation were calculated for six kinds of commercial body and opaque porcelains. The effect of the heating rate on the instantaneous coefficient of thermal expansion was also measured. Tg onset was graphically determined using data on thermal deformation and agreed well with the strain point as defined by viscosity. The data gathered in this study was also compared to the experimental results of previous works by others.

Dental Porcelain↗
PubMed1993

Enhanced chemical strengthening of feldspathic dental porcelain.

Previous studies on ion exchange of dental ceramics have shown that the biaxial flexural strength can be improved by exchanging potassium for sodium ions at temperatures below the strain point. The rubidium ion is bigger than the potassium ion and can also be considered as a candidate for replacing smaller ions, i.e., sodium or potassium, although it has not been used for dental ceramics. The double-step method uses the exchange of a small ion for a large ion (Li for Na) above the strain point, and the further exchange of a large ion for a small ion (K for Li) below the strain point. The purpose of this study was to compare the effect of rubidium-for-potassium ion exchange with that of potassium-for-sodium exchange (Tuf-Coat, G-C International Corp., Japan) on the flexural strength of a feldspathic dental porcelain and to test the hypothesis that a double-step ion exchange can lead to greater strengthening than potassium ion exchange alone. Weight measurements were performed before and after treatment. Qualitative chemical analyses allowed the rubidium, potassium, and sodium concentration profiles to be determined along cross-sections of the specimens. The maximum biaxial stresses were calculated after specimens were fractured in water on a ball-on-ring fixture at 0.5 mm/min. Relative to the untreated control group, the flexural strength of the potassium-exchanged groups was significantly increased, except for those treated at 400 or 500 degrees C. All the groups treated with RbNO3 exhibited a significant increase in flexural strength, with a maximum for the group treated at 450 degrees C.(ABSTRACT TRUNCATED AT 250 WORDS)

Aluminum Silicates↗
PubMed2006

Fracture toughness comparison of three test methods with four dental porcelains.

OBJECTIVE: The aim of this study was to compare three fracture toughness test methods, using four commercial dental porcelains. MATERIALS AND METHODS: The fracture toughness test techniques involved were: the single-edge-notched beam (SENB), the indentation strength method (IS), and a rather convenient ASTM standard for advanced ceramics, which is still rarely used in dental ceramic research, the Chevron-notched beam method (CN). Duceram, Duceram LFC, Sintagon Zx and Carrara Vincent were chosen for study. Data was analyzed by two-way and paired ANOVA. RESULT: No statistical difference was found between the CN and SENB methods with four dental porcelains, but IS was not always in statistical agreement with SENB or CN. Statistical agreement among all three methods occurred only with Duceram LFC. CONCLUSION: The different test methods did not always lead to the same ranking or values of fracture toughness. Yet the toughness results of the SENB method were comparable to those of the CN method for all the four dental porcelains tested in this study.

Analysis of Variance↗
PubMed2006

Archaeological evidence for dental innovation: an eighteenth century porcelain dental prosthesis belonging to Archbishop Arthur Richard Dillon.

During archaeological investigation by Gifford of St Pancras Old Church burial ground, on the eastern edge of Somers Town, London, in advance of construction of the new London terminus for the Channel Tunnel Rail Link, a full porcelain denture was discovered. The high quality porcelain dentures, manufactured in the late eighteenth century French style, may have been brought with their owner, Archbishop Arthur Richard Dillon, on his journey into exile. There is evidence of prolonged use, not only for cosmetic or vocal functions but also in mastication. The dentures are unique archaeological artefacts and represent a pivotal time in dental history, with the adoption of new materials and methods of manufacture. They reflect a period of significant social and economic change for the upper echelons of French society. This paper outlines the development of porcelain dentures, discusses the prosthesis, their owner, and a possible provenance.

Dental Porcelain↗
PubMed1991

Effect of cooling rate on leucite volume fraction in dental porcelains.

Prasad et al. (1988) have shown that slow cooling of dental porcelain produces increases in thermal expansion sufficient to make a compatible metal-porcelain system incompatible. The present study was undertaken to determine whether the increase in porcelain thermal expansion might be attributable to crystallization of additional leucite during slow cooling of the porcelain. Eight x-ray diffraction specimens for each of six commercial dental porcelains and for the Component No. 1 frit of the Weinstein and Weinstein (1962) and Weinstein et al. (1962) patents were fabricated and divided into two groups. Specimens in the first group (termed fast-cooled) were cooled in the conventional manner by removing them from the furnace at the maximum firing temperature immediately into room air. Specimens in the second group (termed slow-cooled) were cooled slowly by interrupting power to the furnace muffle and allowing them to cool inside the closed furnace. Quantitative x-ray diffraction was performed on the fast- and slow-cooled porcelain specimens with standards containing leucite volume fractions of 0.111, 0.223, 0.334, and 0.445. Unpaired, one-tailed t tests were performed on the fast- and slow-cool data, and a significant increase (p less than 0.05) in the amount of leucite (as a function of the slow cooling) was found for each of the porcelains. The increases in the leucite volume fractions resulting from the slow cooling ranged from a low of 8.5% to a high of 55.8%, with an average increase of 26.9%.(ABSTRACT TRUNCATED AT 250 WORDS)

Aluminum Compounds↗
PubMed2001

Determination of elastic properties of metal alloys and dental porcelains.

This study aimed to determine Young's modulus, shear modulus and Poisson's ratio of some metal alloys and dental porcelains used in fixed prosthodontics using the technique of impulse excitation of vibration. It also aimed to compare Young's modulus values of these materials with those obtained using the other two methods: the four-point flexural test and the indentation test using the ultra micro-indentation system (UMIS). Five types of metal alloys and four types of dental porcelains were tested. The samples were prepared to a rectangular shape of approximately 8 x 30 x 1.5 mm. Frequency of vibration in a sample was read when a singular elastic strike was made with an impulse tool. The elastic constants were calculated from the frequency of vibration, dimension and mass of each sample. Young's modulus values resulting from the impulse excitation of vibration are not significantly different (P<0.05) from those obtained using the flexural test and the UMIS test in most metal alloys but are different in titanium, titanium alloy and most of the dental porcelains. The technique of impulse excitation of vibration has proven to be an accurate method and is simple to operate. The elastic properties of these alloys and porcelains are essential for determining the other mechanical properties (fracture toughness) and are relevant in clinical application.

Algorithms↗
PubMed1995

Isothermal anneal effect on leucite content in dental porcelains.

Porcelain thermal expansion behavior is a function of leucite content, and leucite changes can produce porcelain-metal incompatibilities. The purpose of the present study was to determine whether isothermal anneal treatments (such as are encountered during "post-soldering" operations) could result in alterations of leucite content of dental porcelain. Six commercial dental porcelains and the "Component No. 1" frit of the Weinstein et al. patent (1962) were studied. Twenty-eight coupon specimens of each porcelain were fired and divided randomly into seven groups of four specimens each. One group served as a control, while the other six groups were subjected to isothermal anneal treatments--three groups at 500 degrees C and three groups at 750 degrees C, for 4, 8, and 16 min, respectively. Leucite volume fraction was measured via quantitative x-ray diffraction. From an equation for the growth of particles in competition for diffusing material, an expression was derived for the potential simultaneous processes of leucite crystallization and reaction of leucite+glass to form sanidine or other compounds. This exponential growth/decay curve was fit through the experimental data for each porcelain by minimization of the sum of the squares of the residuals through iteration. For each porcelain, a statistically significant correlation was obtained between leucite volume fraction and isothermal anneal duration at 750 degrees C (p < 0.01), whereas at 500 degrees C, only CII exhibited a statistically significant correlation (p < 0.01). The control (non-annealed) leucite volume fractions for the commercial porcelains ranged from (mean +/- SD) 0.155 +/- 0.002 for WIL to 0.442 +/- 0.003 for Component No. 1. The 750 degrees C isothermal anneal increased the leucite volume fraction by between 6.1% and 21.3%.(ABSTRACT TRUNCATED AT 250 WORDS)

Aluminum Silicates↗
PubMed2000

Water-enhanced crystallization of leucite in dental porcelain.

OBJECTIVE: The purpose of this study was to determine whether long-term exposure of dental porcelain to saliva during temporary cementation of a porcelain-fused-to-metal (PFM) restoration could enhance leucite crystallization if the restoration is refired. Such water-enhanced leucite crystallization in dental porcelains could lead to porcelain-metal thermal incompatibility problems. METHODS: Six commercial dental body porcelains and the Component No. 1 (leucite-containing) frit of the Weinstein et al. [13] patent were studied. For each porcelain, 30 coupon specimens were randomly assigned to a treatment group. Ten specimens were placed in artificial saliva, 10 in distilled water, and 10 in a desiccator and were stored for six months. At the end of the six months, an additional 10 coupons of each porcelain were prepared to serve as a control. All 40 specimens of each porcelain were randomized and subjected to one additional firing. Leucite weight fraction was determined by quantitative X-ray powder diffraction analysis via an internal standard technique. RESULTS: Comparisons among the treatments via the least-squares-means test-adjusting for porcelain showed that the saliva group mean leucite weight fraction was significantly higher than that of the other groups. The change in porcelain thermal expansion that would be associated with a leucite change in this range would be between 0.2 x 10(-6) K-1 and 0.3 x 10(-6) K-1. SIGNIFICANCE: The results of this work constitute the first demonstration that moisture absorbed by a porcelain can act as a glass modifier and enhance the crystallization of the glass during subsequent firing. The effect was sufficiently large to generate thermal expansion changes that would exceed the maximum safe mismatch between porcelain and metal.

Absorption↗
PubMed2005

Correlation between fracture toughness and leucite content in dental porcelains.

OBJECTIVES: To determine the correlation between fracture toughness and leucite content in dental porcelains. The mechanisms by which leucite influences the fracture toughness of dental porcelains were also investigated. METHODS: Six porcelains were tested: A (Ceramco I/Dentsply), B (Ceramco II/Dentsitply), C (Finesse/Dentsply), D (d.Sign/Ivoclar), Cb (Cerabien/Noritake) and V (Vitadur Alpha/Vita). Bar-shaped specimens were produced, and their fracture toughness was determined by means of the single-edge precracked beam (SEPB) method. The test consisted of fracturing the specimen after a precrack was generated by a bridge-anvil device. KIc was calculated based on fracture force and size of the precrack. Microstructural analysis and determination of the leucite volume fraction were performed on polished specimens etched with 2% HF for 15s by means of scanning electron microscopy. Fractographic analysis was performed on fracture surfaces. RESULTS: Porcelains A and B presented the highest leucite contents (22%) and similar KIc values (1.23 and 1.22 MPa m1/2, respectively), significantly higher than the other materials. Porcelains C and D presented similar K(Ic) values (0.81 and 0.93 MPa m1/2, respectively), but different leucite contents (6 and 15%, respectively). Porcelain D presented higher KIc compared to porcelains Cb and V (0.71 and 0.75 MPa m1/2, respectively), which presented similar values and the lowest leucite contents (0%). Fractographic analysis showed that porcelains with higher leucite content presented higher incidence of crack deflection. CONCLUSIONS: For the materials evaluated in this study, the leucite content was directly related to KIc. The main toughening mechanism observed was crack deflection around leucite particles and clusters.

Aluminum Silicates↗
PubMed1990

Polished versus autoglazed dental porcelain.

This study compared the finishes on dental porcelain polished with four different polishing paste systems with oven reglazing and with a porcelain adjustment kit without a polishing paste. The polished/reglazed samples were rated according to quality of finish by independent observers and by scanning electron microscopy. On the basis of visual examination, two of the polishing paste systems tested were found to produce a surface equal to or better than oven glazing. On the basis of SEM examination, oven glazing was found to produce a better surface than the other polishing methods. Not all porcelain polishing systems produce a surface comparable to oven-glazed porcelain, and porcelain polishing systems should be chosen carefully.

Dental Polishing↗