PubMed Health⌕ Search

SEARCH · PubMed Health

Results for “DRUG ADULTERATION”

Explore indexed PubMed citations for clinical trials, systematic reviews and public health research. Read source abstracts and follow each citation to its original PubMed record.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 19 recordsLinked to original sources

Dependence on phenobarbital but not pentobarbital using drug-adulterated food.

A drug-adulterated food (DAF) method was used in an attempt to establish physical dependence on either pentobarbital or phenobarbital in male CF1 mice. The mice were acclimated to the control diet for four days and then assigned to treatment groups. Group I continued to receive the control diet; Group II received pentobarbital, 5 mg/g food, increased by 5 mg, daily, for 14 days; Group III received pentobarbital, 5 mg/g food, increased by 5 mg, daily, for 7 days; Group IV received pentobarbital, 10 mg/g food, increased by 10 mg, daily, for 7 days; Group V received phenobarbital at 2.5 mg/g food for 5 days and then 3.0 mg/g food for 2 days. During drug administration, all mice were monitored daily for signs of intoxication, change in body weight, and food consumption. At the end of the drug exposure period all mice received control diet and were observed for signs of withdrawal. Mice in Group II and Group IV demonstrated significant declines in body weight and food consumption and an apparent increase in the degree of intoxication but not signs of withdrawal. Group III mice demonstrated little sign of impairment during exposure to pentobarbital and no withdrawal syndrome was observed. Mice presented phenobarbital were found to exhibit a significant degree of intoxication and a withdrawal syndrome was demonstrated. The data suggest, with respect to the drug administration schedules used, that the DAF method was not suitable for the establishment of physical dependence on pentobarbital in mice.

Animals↗

Drug adulteration.

Explore the source record for details and available documents.

Drug Contamination↗

Analysis of synthetic anti-diabetic drugs in adulterated traditional Chinese medicines by high-performance capillary electrophoresis.

Four synthetic anti-diabetic drugs, acetohexamide (ACE), chlorpropamide (CHL), glibenclamide (GLI) and tolbutamide (TOL), which can be found as adulterants in traditional Chinese medicines (TCMs) were assayed simultaneously using high-performance capillary electrophoresis (HPCE) in 4 min with UV detection at 200 nm. The electrolyte was a buffer solution containing 100 mM phosphate buffer (NaH2PO4/Na2B4O7, pH 7.5). Applied voltage was 15.0 kV and temperature was 30 degrees C. 2-(4-Hydroxyphenyl) ethyl ammonium chloride (HEA) was used as an internal standard. The effects of buffer concentration, pH and supplied voltage on separation were investigated. The relative standard deviations (R.S.D.) of these anti-diabetic drugs for intra-day and inter-day analyses were 0.23-4.27 and 1.23-6.33%, respectively. The recoveries of the synthetic drug adulterants in traditional Chinese medicinal formula ranged from 81.3 to 105.5%. GLI was found and determined in a real sample of TCM.

Buffers↗

Analysis of synthetic chemical drugs in adulterated Chinese medicines by capillary electrophoresis/electrospray ionization mass spectrometry.

Sixteen synthetic chemical drugs, often found in adulterated Chinese medicines, were studied by capillary electrophoresis/UV absorbance (CE/UV) and capillary electrophoresis/electrospray ionization mass spectrometry (CE/ESI-MS). Only nine peaks were detected with CZE/UV, but on-line CZE/MS provided clear identification for most compounds. For a real sample of a Chinese medicinal preparation, a few adulterants were identified by their migration times and protonated molecular ions. For coeluting compounds, more reliable identification was achieved by MS/MS in selected reaction monitoring mode. Micellar electrokinetic chromatography (MEKC) using sodium dodecyl sulfate (SDS) provided better separation than capillary zone electrophoresis (CZE), and, under optimal conditions, fourteen peaks were detected using UV detection. In ESI, the interference of SDS was less severe in positive ion mode than in negative ion mode. Up to 20 mM SDS could be used in direct coupling of MEKC with ESI-MS if the mass spectrometer was operated in positive ion mode. Because of better resolution in MEKC, adulterants can be identified without the use of MS/MS.

Anti-Inflammatory Agents↗

[Lead poisoning due to drug addiction: a new source of poisoning with clinical interest and important epidemiological consequences].

Lead poisoning has accompanied the human being throughout history. Owing to the increasing levels of safety at work, the incidence of occupational poisoning has decreased and new forms of non-occupational poisoning have emerged. We present 3 cases of drug addicts, with lead poisoning, as a result of using adulterated drugs. One of them was an intravenous drug addict who had abdominal pain and anemia. The other 2 inhaled heroin, one being slightly anemic and the other without symptoms and with normal hemoglobin levels. The drug adulterated with lead had not been previously recognized as a source of lead poisoning, being likely to cause serious epidemiological effects.

Adult↗

Identification of prescription drugs in adulterated Chinese herbal medications.

Analytical difficulties involved in the detection of a wide range of suspected polar and nonpolar drugs in botanical matrices have been solved by adopting a multipronged approach. Preliminary screening of Chinese herbal medications can be accomplished by a combination of thin-layer chromatography and gas chromatography/mass spectrometry and/or the employment of liquid chromatography/mass spectrometry as a probe introduction technique.

Chromatography, Liquid↗

Chemical data: an essential tool in the regulation of drugs.

How the Bureau of Drugs laboratories and offices obtain chemical data from the scientific literature, from user complaints and product defect reporting systems, from the drug manufacturers, from analyses of drug samples collected from the market, and from analytical research are described. The chemical data thus educed have been used successfully in developing new analytical methods, in establishing better specifications of drug quality, in removing adulterated drugs from the marketplace, in successfully prosecuting purveyors of substandard drugs, and in general assuring that consumers are provided with safe and effective drugs of high quality.

Biopharmaceutics↗

Lichenoid drug eruption: crystal methamphetamine or adulterants?

Many drugs have been reported to produce an eruption that is clinically and histologically indistinguishable from lichen planus. I report a case of lichenoid drug eruption occurring after crystal methamphetamine abuse. To my knowledge, this is the first report of an illicit drug causing a lichenoid drug eruption.

Adult↗

Two deaths resulting from apparent parenteral injection of strychnine.

Large amounts of strychnine were found in the bodies of two drug abusers, presumable as a result of injection of "street drugs" adulterated with strychnine. Current therapeutic research with this drug, if widely accepted into medical practice, may lead to its greater availability and hence an increased poisoning incidence potential.

Adolescent↗