Biomedical subjects
Publications and source records attributed to B Unterhalt.
3-Methyl-4-thia-cyclohexylsulfamic acid was synthesized, the degree of sweetness of its sodium salt was measured, and compared with that of the sodium salts of 3-methyl-cyclohexylsulfamic acid, 4-thia-cyclohexylsulfamic acid, and cyclohexylsulfamic acid.
Saccharin may be determined by gas chromatography after methylation with diazomethane. In this reaction there are found N-methyl-saccharin, and the O-methyl ether as well as methoxycarbonyl benzenesulfonamide by ring fission.
The sodium salts of cis- and trans-2-methyl-cyclohexylsulfamic acid were synthesized and tasted. There is no difference in their degree of sweetness.
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