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PubMedDate not supplied

A simple method to obtain essential oils from Salvia triloba L. and Laurus nobilis L. by using microwave-assisted hydrodistillation.

A microwave-assisted hydrodistillation protocol was modified to extract essential oils from leaves of Salvia triloba L. and Laurus nobilis L. The essential oils of these plants are generally obtained by hydrodistillation or steam distillation. The volatile compounds obtained by microwave-assisted hydrodistillation and hydrodistillation methods were analyzed by GC and GC/MS. Both distillation methods and analytical results were compared. 1,8-Cineole (46.8-54.2%) was the main component in the leaf oils of both samples. Although the distillation was accomplished in a shorter time, oil yields and 1,8-cineole contents were slightly higher in the microwave-assisted hydrodistillation compared to usual hydrodistillation. Microwave-assisted hydrodistillation appears to be an effective method for the production of essential oils.

Laurus↗

PubMed1990

Social occasions and the perceived appropriateness of consuming different alcoholic beverages.

Based on a national probability sample of 2,401 Americans aged 21 and over (1,069 of whom were deemed "drinkers" on the basis of having drunk at least one alcoholic beverage within the previous 7 days), this study looks at differences in the perceived situational appropriateness of drinking beer, distilled spirits, wine and wine coolers in each of six social occasions. It was found that wine is usually deemed appropriate in integrative, social enjoyment-enhancing situations. Beer use tends to be viewed ambivalently, with a sort of "cross-situational neutrality"; its use is neither strongly condoned nor strongly condemned in any of the six social contexts under study. People's attitudes toward the use of distilled spirits are best described as allowing for a "cautious indulgence" in this beverage. The respondents tend to favor drinking distilled spirits during integrative social occasions, feel ambivalently toward drinking in social contexts that are simultaneously integrative and disintegrative and disfavor drinking during disintegrative and anxiety-reductive social occasions. Wine cooler use is viewed inconsistently, perhaps with a tendency toward being seen as appropriate for consumption during integrative social occasions that involve having a good time. Sex, income and marital status differences were found to be minimal. Age, though, was found to be a discerning variable in many of these relationships, such that people aged 65 or older were less likely than their younger counterparts to endorse drinking in all of the social contexts under study, except for drinking as a perfect complement to a nice dinner.

Adult↗

PubMed2000

A moderate intake of wine is associated with reduced total mortality and reduced mortality from cardiovascular disease.

OBJECTIVE: The aim of this study was to investigate the effects of the consumption of wine, beer and distilled spirits on total mortality and on mortality from cardiovascular disease. METHOD: The consumption of wine, beer and distilled spirits was assessed in 1,828 individuals by a psychiatrist. Subjects were selected according to expected level of need for health services, from a random sample of 24,043 individuals aged 18-65 years. Mortality was recorded after 22 years and the results related to those for the individuals not exposed to the factor examined. The results were adjusted for age, expected level of need for health services, total alcohol consumption, gender, body-mass index, tobacco use and social class. RESULTS: Intake of wine once a week or more (compared with intake of wine less than once a week or not at all) was associated with a relative risk ratio of 0.58 for total mortality (95% CI: 0.40-0.84) and a relative risk ratio of 0.49 for mortality from cardiovascular disease (95% CI: 0.27-0.90). The risk reduction seemed to be confined to those consumers of wine who had an intake of less than 140 grams of alcohol per week and consumed the beverage once a week. Ex-drinkers had an increased relative risk ratio in total mortality compared with lifelong abstainers and individuals who consumed less than 50 grams of alcohol per week (relative risk ratio = 2.64; 95% CI: 1.56-4.49). CONCLUSIONS: A low to moderate intake of wine seems, unlike the consumption of distilled spirits and beer, to be associated with reduced total mortality and reduced mortality from cardiovascular disease.

Adolescent↗

PubMed2006

Alcohol consumption, alcoholics anonymous membership, and suicide mortality rates, Ontario, 1968-1991.

OBJECTIVE: The goal of this study is to identify alcohol-related factors that influence mortality rates from suicide. Specifically, we examine the impact of per capita consumption of total alcohol, distilled spirits, and beer and wine; unemployment rate; and Alcoholics Anonymous (AA) membership rate on total and male and female suicide mortality rates in Ontario between 1968 and 1991. METHOD: We studied the impact of alcohol consumption levels, AA membership rates, and unemployment rates on suicide mortality rates in Ontario from 1968 to 1991. Time series analyses with Auto Regressive Integrated Moving Average (ARIMA) modeling were applied to total and male and female suicide rates. The analyses performed included total alcohol consumption, distilled spirits consumption, beer consumption, and wine consumption. Missing AA membership data were interpolated with cubic splines. RESULTS: Total alcohol consumption and consumption of each of beer, distilled spirits, and wine were significantly and positively related to total and female suicide mortality rates. AA membership rates were negatively related to total and female suicide rates. Although data for males did not reach significance (except for the relationship between wine consumption and suicide rate), the direction of effects was consistent with that observed for female and total suicide rates. Unemployment rates were positively related to male and total suicide rates in some models. CONCLUSIONS: These data confirm the important relationships between per capita consumption measures and suicide mortality rates seen by previous investigators. Additionally, the results for AA membership rates are consistent with the hypothesis that AA membership and treatment for misuse of alcohol can exert beneficial effects observable at the population level.

Adolescent↗

PubMed2006

The impact of alcohol taxation on liver cirrhosis mortality.

OBJECTIVE: The objective of this study is to investigate the impact of distilled spirits, wine, and beer taxes on cirrhosis mortality using a large-panel data set and statistical models that control for various other factors that may affect that mortality. METHOD: The analyses were performed on a panel of 30 U.S. license states during the period 1971-1998 (N = 840 state-by-year observations). Exogenous measures included current and lagged versions of beverage taxes and income, as well as controls for states' age distribution, religion, race, health care availability, urbanity, tourism, and local bans on alcohol sales. Regression analyses were performed using random-effects models with corrections for serial autocorrelation and heteroscedasticity among states. RESULTS: Cirrhosis rates were found to be significantly related to taxes on distilled spirits but not to taxation of wine and beer. Consistent results were found using different statistical models and model specifications. CONCLUSIONS: Consistent with prior research, cirrhosis mortality in the United States appears more closely linked to consumption of distilled spirits than to that of other alcoholic beverages.

Alcoholic Beverages↗

PubMed1981

[A modified FEP (free erythrocyte protoporphyrin) test (author's transl)].

In order to simplify FEP (free erythrocyte protoporphyrin) test, we studied on the Piomelli's method, specially on the preparation of standard solution and on the role of celite-saline. N,N-dimethylformamide (DMFA) was used as the solvent of protoporphyrin standard (protoporphyrin IX dimethylester, Sigma Chemical Co.). The stock solution was stable for over 6 months at 4 degrees C. To examine the recovery and extraction efficiency, the stock solution (PP) diluted with DMFA was also added to blood. Ten microliter of DMFA added to 40 microliter blood had no effect on the FEP extraction. In the absence or at low concentrations of protein components, fluorescence intensity of added protoporphyrin extremely decreased in the extract with celite-saline. It seems to be due to the adsorption of protoporphyrin to celite. In the presence of proteins, there was no difference between fluorescence intensity of protoporphyrin with celite-saline dilution extraction and that with distilled water dilution extraction. The FEP levels in 128 lead workers (blood lead levels, 4.9-80.8 micrograms/100 g) with celite-saline extraction were almost the same as with distilled water dilution extraction. Thus celite-saline dilution was able to be displaced by the distilled water dilution, and the extraction procedure was slightly simplified. With our method, the average recovery was 93% and extraction efficiency was 80-90%.

Dimethylformamide↗

PubMed1999

Contact angle measurement on dental implant biomaterials.

Wettability may be one of the surface factors to be considered when selecting dental implant biomaterials. Contact angles of dental implant surface preparations influence wettability and tissue adhesion. The contact angles of eight implant surface preparations were determined in this study. Contact angles were measured by a tele-microscope equipped with a protractor eyepiece. Groups 1 to 6 had a Ti6Al4V substrate. Group 1 was metallurgically polished, group 2 was blasted with 180 microns Al2O3, group 3 was blasted with 710 microns Al2O3, group 4 was hydroxyapatite (HA) blasted (125 microns), group 5 had a Calcitite HA plasma-sprayed coating, and group 6 was coated with plasma-sprayed MP-1 HA. Group 7 was metallurgically polished commercially pure (CP) titanium (grade 1), and group 8 was etched CP titanium (grade 1). Contact angles were measured 30 times for each group with distilled water and glycerol, and the determinations were statistically analyzed. Mean contact angles for groups 1 to 8 were 65.5, 65.3, 62.5, 67.9, 46.6, 81.7, 58.5, and 69.0, respectively, when tested with distilled water, and 70.7, 68.3, 81.6, 75.4, 67.1, 70.7, 62.3, and 82.5, respectively, when tested with glycerol. Analysis of variance and Tukey's Honestly Significant Difference test (p = 0.05) demonstrated significant differences between group 5 and all other groups when groups were tested with distilled water and demonstrated no significant differences between groups 5 and 7 when groups were tested with glycerol. Surface preparation of implant biomaterials affects wettability. In this study, Ti6Al4V coated with Calcitite HA had the lowest contact angles and the best wettability.

Alloys↗

PubMed2002

Chemical stimuli from corn plants affect host selection and oviposition behavior of Sesamia nonagrioides (Lepidoptera: Noctuidae).

The role of chemical stimuli in host selection and oviposition of Sesamia nonagrioides (Lef) was studied in the laboratory using eight corn hybrids. Female oviposition preference was evaluated on plants of the eight hybrids, their extracts in pentane and methanol, and volatiles collected by steam distillation in ether. Results from two-choice bioassays indicate various degrees of female preference to the hybrids. Four hybrids received more eggs than control plants, whereas the remainder received fewer eggs. Relatively similar results were obtained when filter paper sticks baited with pentane and steam distillation extracts were evaluated. Methanol extracts from all eight hybrids received fewer eggs than the methanol controls. Results showed that pentane and steam distillation extracts contain chemicals that elicit female oviposition response, while methanol extracts may contain chemicals that deter or repel females to oviposition.

Animals↗

PubMed2006

Acaricidal activities of extracts of Kochia scoparia against Tetranychus urticae, Tetranychus cinnabarinus, and Tetranychus viennensis (Acari: Tetranychidae).

Extracts of an annual herbaceous plant, Kochia scoparia (L.) Schrad (Macrophomina), were bioassayed to determine their acaricidal activities against Tetranychus urticae Koch, Tetranychus cinnabarinus (Boisduval), and Tetranychus viennensis Zacher (Acari: Tetranychidae) in the laboratory. Extracts had both contact and systemic toxicity to these mites. Three solvents were tested for preparing crude extracts: petroleum ether, chloroform, and methanol. Methanol was the most effective solvent, extracting 3.11-4.53% of the acaricide. Petroleum ether was the least effective solvent, extracting 1.25-1.54%. However, extracts with chloroform resulted in the highest mite mortality (78.86%), and ultrasound-assisted extraction required the least time (10 min). Concentrated extracts were prepared using chloroform, methyl acetate, or distilled water as a solvent. Mite mortalities from the concentrated extracts by methyl acetate or distilled water were significantly lower than those by chloroform. The mean lethal concentrations (LC50) of the extracts by chloroform, methyl acetate, and distilled water to the mites were 0.71 +/- 0.06, 2.08 +/- 0.16 and 8.75 +/- 0.062 mg/ml, respectively. After liquid chromatography and thin layer chromatography, the concentrated extracts by chloroform were separated into seven groups of isolated fractions and tested for acaricidal activity.

Animals↗

PubMedDate not supplied

Effects of atorvastatin on vascular remodeling in spontaneously hypertensive rats.

OBJECTIVE: To investigate the structural changes of aorta, and evaluate the effects of atorvastatin on the remodeling of thoracic aorta in spontaneously hypertensive rats (SHR). METHODS: Twelve eight-week-old SHR were randomized into atorvastatin treated group (ATV group, n=6) and distilled water group (DW group, n=6); Wistar-Kyoto rats (WKY) were used as normal controls. Atorvastatin was administered to ATV group for 10 weeks by gavage in mixture with distilled water (1 ml); the latter two groups were given the same amount of distilled water by gavage for 10 weeks. Systolic blood pressure of caudal artery was examined before and after treatment, and serum concentrations of total cholesterol, triglycerides and HDL-C were measured. Wall thickness, media thickness, medial cross-sectional area and lumen diameter of thoracic aorta were assessed with computed video processing. RESULTS: Systolic blood pressure in ATV group was markedly lower than that in DW group (P<0.01). Compared with DW group and WKY group, serum concentrations of total cholesterol, triglycerides and HDL-C in ATV group were significantly lower (P<0.01,P<0.05). Wall thickness, media thickness, and medial cross-sectional area to lumen ratio in DW group were significantly higher than those in WKY group and ATV group (P<0.01,P<0.05), but no such difference was found between WKY group and ATV group (P>0.05). CONCLUSION: Vascular structural changes of aorta are due to the alteration of the vessel wall in early stage of SHR. Atorvastatin can markedly improve vascular remodeling.

Animals↗

PubMedDate not supplied

Effect of BioSentry 904 and ethylenediaminetetraacetic acid-tris disinfecting during incubation of chicken eggs on microbial levels and productivity of poultry.

Proper sanitation practices and the use of efficacious disinfectants in a hatchery have an effect on chick quality. Aerosol bacterial counts, egg moisture loss, hatchability, chick quality, and broiler productivity were evaluated when egg surfaces were contaminated by immersion of each egg into a broth medium containing a field isolate of Pseudomonas aeruginosa and incubated with exposure to one of three disinfectant treatments administered by fine spray: distilled water, BioSentry 904 (904), and a 1:1 ratio of 904 and ethylenediaminetetraacetic acid (EDTA)-Tris. The aerosol bacteria levels were statistically greater on day 21 of incubation in the group treated with distilled water than in those receiving disinfectants. Overall hatch of fertile eggs and egg moisture loss were comparable among all three treatments. At 1 day of age, the chicks incubated with 904 had a statistically lower yolk sac contamination rate than those incubated with 904+EDTA-Tris or distilled water. The 2-wk mortality rates, body weights, feed conversion ratios, yolk sac weights, and yolk sac contamination rates were all similar among the three treatments.

Animals↗

PubMed1984

Relative error (variability) associated with an improved instrument for measuring gingival crevicular fluid.

This investigation was undertaken to compare the variability in a new Periotron model 6000 to the variability in the previous Periotron model 600 and to the variability of the ninhydrin area method (NAM) for measuring quantities of fluid collected on filter paper strips. A Hamilton microliter syringe was used to deliver normal human serum to filter paper strips. Strips receiving varying quantities were randomly and blindly assigned to Periotron models 6000 and 600 until 10 strips containing each of 0.15, 0.30, 0.45, 0.60, 0.75, 0.90 and 1.05 microliter had been read using model 6000 and 10 strips containing each of 0.15, 0.30 and 0.45 microliter had been read using model 600. All strips were subsequently read using the NAM. The entire procedure was repeated using distilled water containing 0.1% methyl green. Coefficients of variation (CV) were computed for all sets of data. In all cases the CVs for the Periotron 6000 were significantly smaller than those for the Periotron 600 or the NAM. Pooled estimates of CVs (0.15-0.45 microliter) for the Periotron models 6000 and 600 were 0.054 and 0.116, respectively, (P less than or equal to 0.005) with serum and 0.059 and 0.095, respectively, (P less than or equal to 0.05) with distilled water containing 0.1% methyl green. Pooled estimates of CVs (0.15-1.05 microliter) for the Periotron model 6000 and the same strips subsequently measured with the NAM were 0.046 and 0.069, respectively, (P less than or equal to 0.005) with serum and 0.055 and 0.076, respectively, (P less than or equal to 0.001) with distilled water containing 0.1% methyl green.(ABSTRACT TRUNCATED AT 250 WORDS)

Equipment Design↗

PubMed1989

Effects of potassium oxalate on dentin hypersensitivity in vivo.

This study compared 30% dipotassium oxalate (DO) and 3% monohydrogen-monopotassium oxalate (MO) on the reduction of dentin hypersensitivity in vivo. Four treatments were utilized: (1) distilled water followed by 30% DO; (2) distilled water followed by 3% MO; (3) 30% DO followed by 3% MO and (4) distilled water only. Treatments were randomly assigned so that each of the 17 participants received all four treatments, one per tooth tested. Response to cold at baseline and immediately, 1 week, 2 weeks, and 4 weeks posttreatment was measured. Testing began with water at 20 degrees C and decreased at 5 degrees C intervals until a positive response was obtained or until 0 degrees C was reached. No differences were found for time when compared across treatments. When treatments were compared across time, significant reductions occurred in immediate and 4 week posttreatment measurements for treatment 2. In addition, highly significant reductions occurred in 1 week and 2 week posttreatment measurements for treatment 3. Results suggest a decrease in dentin hypersensitivity following the application of 3% MO alone, and 30% DO followed by 3% MO.

Adult↗

PubMed1989

Carcinogenicity of dark liquor.

To investigate whether the non-alcohol content of distilled alcoholic beverages affects the carcinogenicity of the beverage, we conducted an epidemiologic study of laryngeal and hypopharyngeal cancer. We interviewed 384 cases (or spouses, for deceased cases), and compared their responses with those of 876 controls. We classed distilled liquors as dark or light, a rough division according to content of potentially carcinogenic compounds in the beverages. The relative effect on hypopharyngeal cancer risk was much stronger for those who reported high consumption of dark liquor (relative risk = 4.4, 90% confidence interval = 2.9, 6.8) than for those reporting comparable consumption of light liquor (relative risk = 1.3, 90% CI = 0.8, 2.1). For laryngeal cancer, consumption of dark liquor had a smaller effect, and there was little distinction between the effects of dark and light liquor. The data appear consistent with the theory that the non-alcoholic content of distilled alcoholic beverages is a determinant of cancer risk, and that alcoholic beverages act topically rather than systemically in their carcinogenic action.

Alcoholic Beverages↗

PubMed1983

The recovery period of the taste responses of rat chorda tympani after application of toothpaste.

The recovery period of the taste responses of rat chorda tympani after application of toothpaste was examined. The response observations of four kinds of essential taste stimuli, 0.1 M sodium chloride, 0.005 M quinine hydrochloride, 1.0 M sucrose, and 0.05 M tartaric acid, were repeated every 2 or 5 minutes. After five observations of summated responses of the chorda tympani with each taste stimulus, a toothpaste solution diluted 3 to 1 was applied to rat tongues for 3 minutes and then they were washed with distilled water for 1.5 minutes. Thereafter, observations of the responses to each taste stimulus were repeated at 2 or 5 minute intervals for 30 or 60 minutes. The responses caused by four kinds of essential taste stimuli became smaller immediately after application of toothpaste, and then gradually returned to normal. The same experimental procedure was also applied using an application of distilled water instead of an application of toothpaste to rat tongues. A t-test was performed between the response ratios after application of toothpaste and those after application of distilled water. Significant differences disappeared at 18 minutes after application on the 0.1 M sodium chloride stimulus, at 23 minutes on the 0.005 M quinine hydrochloride stimulus, at 15 minutes on the 1.0 M sucrose stimulus, and at 15 minutes on the 0.05 M tartaric acid stimulus. The authors estimated that all kinds of taste responses recovered within at least 50 minutes.

Animals↗

PubMedDate not supplied

Simplified method for detecting tritium contamination in plants and soil.

Cost-effective methods are needed to identify the presence and distribution of tritium near radioactive waste disposal and other contaminated sites. The objectives of this study were to (i) develop a simplified sample preparation method for determining tritium contamination in plants and (ii) determine if plant data could be used as an indicator of soil contamination. The method entailed collection and solar distillation of plant water from foliage, followed by filtration and adsorption of scintillation-interfering constituents on a graphite-based solid phase extraction (SPE) column. The method was evaluated using samples of creosote bush [Larrea tridentata (Sessé & Moc. ex DC.) Coville], an evergreen shrub, near a radioactive disposal area in the Mojave Desert. Laboratory tests showed that a 2-g SPE column was necessary and sufficient for accurate determination of known tritium concentrations in plant water. Comparisons of tritium concentrations in plant water determined with the solar distillation-SPE method and the standard (and more laborious) toluene-extraction method showed no significant difference between methods. Tritium concentrations in plant water and in water vapor of root-zone soil also showed no significant difference between methods. Thus, the solar distillation-SPE method provides a simple and cost-effective way to identify plant and soil contamination. The method is of sufficient accuracy to facilitate collection of plume-scale data and optimize placement of more sophisticated (and costly) monitoring equipment at contaminated sites. Although work to date has focused on one desert plant, the approach may be transferable to other species and environments after site-specific experiments.

Cost-Benefit Analysis↗

PubMed2006

Measuring runoff-suspended solids using an improved turbidometer method.

Differences in particle size distribution between runoff standards and unknown samples affect the accuracy of estimation of total suspended solids (TSS) concentration using the nephelometric turbidity (NTU) method. The objective was to quantify the effects of a sucrose solution as suspending medium and contrasting particle size distribution on nephelometric turbidity and accuracy of TSS estimation. Nineteen benchmark soils varying in texture and color were divided into particle size distribution of <250 and <2000 microm. Soils from these two aggregate classes were then made into suspension ranging from 0.2 to 15 g L-1 using distilled deionized water. Runoff suspensions ranging from 0.2 to 21 g L-1 were also collected from different watersheds. Turbidity of soil and runoff suspensions was measured in sucrose solution and in distilled deionized water. The sucrose solution density ranged from 1.10 to 1.30 kg L-1. Increasing sucrose solution density decreased turbidity. The TSS concentration was most sensitive to changes in turbidity with the 1.30 kg L-1 sucrose solution. Using the 1.30 kg L-1 sucrose solution, particle size bias and error of TSS estimates were decreased by at least 20% compared to distilled deionized water. Reduction in refraction index differences between the suspended particles and sucrose solution combined with reduced particle settling and reduced Brownian motion resulted in dampening the effects of particle size distribution. We propose a sucrose solution of 1.30 kg L-1 as a better suspending medium to dampen the effect of particle size distribution and thus improve suspension TSS concentration estimation.

Nephelometry and Turbidimetry↗

PubMed2005

Survival of Lactobacillus plantarum 44a after spraying and drying in feed and during exposure to gastrointestinal tract fluids in vitro.

A good probiotic strain should be able to survive the conditions of handling and storage to be delivered in high concentration to the host. That is especially important when stressful conditions are prevalent in the carrier, for instance in low water content foods like animal feed. The aim of this research was to study the survival of the probiotic candidate Lactobacillus plantarum 44a after spraying and drying in feed, and during storage and exposure to gastrointestinal tract fluids in vitro. In addition, the viability of the strain during exposure to distilled water and 2% NaCl was studied. Feed was sprayed with a suspension of asymptotically equal to 2 x 10(10) CFU of L. plantarum 44a in 10, 15, 20, 25 and 30% v/w of the feed and dried to constant weight (6% moisture) in a convective oven at 25 degrees C. L. plantarum 44a survived 14.67, 36, 51.86, 78.9 and 105.3% respectively in relation to the original % v/w of the feed. After 3 weeks of storage at 25 degrees C, survival was similarly low in all the treatments. L. plantarum 44a stored in feed containing 13% moisture, vacuum-packaged and stored in refrigeration, maintained high viability (approximately 100%) after 1 year of storage. Survival was not affected after feed-containing lactobacilli was exposed to gastrointestinal fluids in a simulation model. Viability of L. plantarum 44a as a cell suspension in PBS added directly to distilled water or distilled water with 2% NaCl was maintained up to 48 h; after 72 h, viability started to decline. It is concluded that L. plantarum 44a maintained high viability after being dried and stored in feed even after exposure to gastric and intestinal fluids in vitro.

Animal Feed↗