PubMed · 232263
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W Jakubowski, W Graban, M Kazoń, S Zurowski. [Renal angioscintigraphy (author's transl)].. https://pubmed.ncbi.nlm.nih.gov/232263/
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The first total synthesis of the natural cytotoxic agent sporiolide A has been accomplished from D-glucal in 16 steps with 6.1% overall yield. Carbohydrates were applied as the chiral templates to manipulate the absolute configuration during the synthesis. Pyridinium chlorochromate (PCC)-promoted transformation of the cyclic enol-ether to lactone, followed by Yamaguchi esterification and intramolecular ring closure metathesis, greatly facilitates synthesis of the target compound.
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